1,2,3,4,6-戊-O-乙酰基-beta-D-(C1-2H)吡喃葡萄糖合成路线 （共 6 条）
反应条件
1: 2,3,4,6-tetra-O-acetyl-D-glucono-1,5-lactone With sodium borodeuteride; water-d2 in tetrahydrofuran
T=0°C;
2: acetic anhydride in tetrahydrofuran
T=20°C; 0.5 h; Further stages.;
参考文献
Indurugalla; Bennet
Journal of the American Chemical Society, 2001 , vol. 123, # 44 p. 10889 - 10898
反应条件
sodium borodeuteride in tetrahydrofuran; water-d2
1.) 0 deg C, 1 h, 2.) RT; overnight,;
参考文献
Berven, Leise A.; Withers, Stephen G.
Carbohydrate Research, 1986 , vol. 156, p. 282 - 285
反应条件
in pyridine
T=20°C; 72 h; Cooling with ice; Overall yield = 96 percent; Overall yield = 62 mg;
参考文献
Perez-Hernandez, Nury; Alvarez-Cisneros, Celina; Cerda-Garcia-Rojas, Carlos M.; Morales-Rios, Martha S.; Joseph-Nathan, Pedro
Magnetic Resonance in Chemistry, 2013 , vol. 51, # 3 p. 136 - 142
反应条件
sodium acetate
Yield given;
参考文献
Funabashi, Masuo; Hasegawa, Toshimori
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2528 - 2531
反应条件
sodium borodeuteride; sodium acetate
1.) pH 5-6; Yield given. Multistep reaction;
参考文献
Funabashi, Masuo; Yoshioka, Shigetake
Chemistry Letters, 1984 , p. 677 - 680
参考文献
Funabashi, Masuo; Yoshioka, Shigetake
Chemistry Letters, 1984 , p. 677 - 680
