N,N-二乙基-3-噻吩羧酰胺合成路线 （共 11 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 24 h; Reflux;
参考文献
Rieke, Reuben D.; Kim, Seung-Hoi
Tetrahedron Letters, 2012 , vol. 53, # 27 p. 3478 - 3481
反应条件
potassium phosphate; PdClMe(1,5-cyclooctadiene) in 1,4-dioxane T=100°C; P=7600 Torr; 15 h;
参考文献
Journal of Organometallic Chemistry, , vol. 687, # 2 p. 436 - 443
反应条件
in dichloromethane 1 h;
参考文献
Kuo, Cheng-Yu; Nie, Wanyi; Tsai, Hsinhan; Yen, Hung-Ju; Mohite, Adytia D.; Gupta, Gautam; Dattelbaum, Andrew M.; William, Darrick J.; Cha, Kitty C.; Yang, Yang; Wang, Leeyih; Wang, Hsing-Lin
Macromolecules, 2014 , vol. 47, # 3 p. 1008 - 1020
反应条件
1: SOCl2 / CHCl3 / 3 h / Heating 2: CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 40, # 11 p. 1585 - 1599
反应条件
in tetrahydrofuran; dichloromethane
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in diethyl ether 1.) -78 deg C, 1 h, 2.) -78 deg C -> RT, 12 h;
参考文献
Journal of the American Chemical Society, , vol. 102, # 4 p. 1457 - 1460
反应条件
n-butyllithium in tetrahydrofuran
参考文献
Doklady Chemistry, , vol. 440, # 1 p. 257 - 262
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine; hydroxycarbonylphosphonic acid 1.) hexane, ether, -78 deg C, 1.5 h, 2.) hexane, ether, a) -78 deg C, 7 h, b) RT, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Acta Chemica Scandinavica, , vol. 47, # 3 p. 318 - 322
反应条件
N,N,N',N,-tetramethylethylenediamine; hydroxycarbonylphosphonic acid 1.) hexane, ether, -78 deg C, 1.5 h, 2.) hexane, ether, a) -78 deg C, 7 h, b) RT, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Acta Chemica Scandinavica, , vol. 47, # 3 p. 318 - 322
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine 1.) hexane, ether, -78 deg C, 1.5 h, 2.) hexane, ether, a) -78 deg C, 7 h, b) RT, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Acta Chemica Scandinavica, , vol. 47, # 3 p. 318 - 322
