2,4-二溴-N-甲基苯胺合成路线 （共 17 条）
反应条件
1: 87 percent / formic acid / H2O / 24 h / Heating 2: 1.) n-BuLi / 1.) THF, hexane, -90 deg C, 20 min, 2.) THF, hexane, from -90 deg C to RT View Scheme
参考文献
Stanetty, Peter; Krumpak, Barbara; Rodler, Inge K.
Journal of Chemical Research, Miniprint, 1995 , # 9 p. 2111 - 2122
反应条件
1-benzyl-1-aza-4-azoniabicyclolt;2.2.2gt;octane bromide; calcium carbonate in methanol
T=20°C; 0.25 h;
参考文献
Hajipour; Imanieh; Pourmousavi
Synthetic Communications, 2004 , vol. 34, # 24 p. 4597 - 4604
反应条件
tetra-n-butylammonium tribromide in chloroform
0.0333333 h;
参考文献
Berthelot, J.; Guette, C.; Essayegh, M.; Desbene, P.L.; Basselier, J.J.
Synthetic Communications, 1986 , vol. 16, # 13 p. 1641 - 1646
反应条件
trifluoroacetic acid
T=20°C; 24 h;
参考文献
Didier, Delphine; Tylleman, Benoit; Lambert, Natacha; Vande Velde, Christophe M.L.; Blockhuys, Frank; Collas, Alain; Sergeyev, Sergey
Tetrahedron, 2008 , vol. 64, # 27 p. 6252 - 6262
反应条件
tert.-butylnitrite; copper(ll) bromide in acetonitrile
T=60°C; 2 h; Product distribution;
参考文献
Doyle, Michael P.; Lente, Michael A. van; Mowat, Rex; Fobare, William F.
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2570 - 2575
参考文献
Fischer,O.
Chemische Berichte, 1912 , vol. 45, p. 1100
反应条件
tert.-butylnitrite; copper(ll) bromide in acetonitrile
T=60°C; 2 h; Product distribution;
参考文献
Doyle, Michael P.; Lente, Michael A. van; Mowat, Rex; Fobare, William F.
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2570 - 2575
反应条件
in acetone
Ambient temperature;
参考文献
Effenberger, Franz; Steinbach, Adalbert; Epple, Gerhard; Hanauer, Johann
Chemische Berichte, 1983 , vol. 116, # 11 p. 3539 - 3551
反应条件
acetate buffer
T=70°C; Ea, ΔS(excit.); var. temp. and reaction partners; Rate constantMechanismThermodynamic data;
参考文献
Kavalek, Jaromir; Kralikova, Ulrika; Machacek, Vladimir; Sedlak, Milos; Sterba, Vojeslav
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 1 p. 202 - 222
参考文献
Esselen; Clarke
Journal of the American Chemical Society, 1914 , vol. 36, p. 321
