2-氯-6-甲基喹啉-3-甲醛合成路线 （共 8 条）
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide; trichlorophosphate in acetonitrile Vilsmeier-Haack cyclisation; 0.75 h; Heating;
参考文献
Ali; Tasneem; Rajanna; Sai Prakash
Synlett, 2001 , # 2 p. 251 - 253
反应条件
trichlorophosphate T=60°C; 16 h;
参考文献
Pawar; Bajare; Mundade
Journal of the Indian Chemical Society, 1990 , vol. 67, # 8 p. 685 - 686
反应条件
1.1: triethylamine / chloroform / 1 h / 0 °C 2.1: trichlorophosphate / 0 - 75 °C / Inert atmosphere 2.2: 0.5 h / 0 - 10 °C / Inert atmosphere View Scheme
参考文献
Heterocyclic Communications, , vol. 17, # 3-4 p. 111 - 119
反应条件
trichlorophosphate T=75°C; 16 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1520 - 1530
参考文献
Heterocycles, , vol. 21, # 2 p. 568
反应条件
hydrogenchloride; water T=90°C;
参考文献
US2008/139558 A1, ;
Page/Page column 54 ;
US 20080139558 A1
反应条件
sodium tetrahydroborate in methanol T=20°C; 0.166667 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 45, # 3 p. 430 - 433
反应条件
1: sodium tetrahydroborate / methanol / 0.5 h / 20 °C
2: thionyl chloride / benzene / 4 h / Reflux
View Scheme
参考文献
Mareddy, Jyoti; Shanthi Praveena, Koduru Sri; Suresh, Nallapati; Jayashree, Anireddy; Roy, Soma; Rambabu, Dandela; Sreenivasa Murthy, Nandula Yadagiri; Pal, Sarbani
Letters in Drug Design and Discovery, 2013 , vol. 10, # 4 p. 343 - 352
