1-(1-羟基-4-甲氧基-2-萘)-乙酮合成路线 （共 21 条）
反应条件
in dichloromethane
T=0°C;
参考文献
Chen, You-Sheng; Kuo, Pei-Yu; Shie, Tien-Lan; Yang, Ding-Yah
Tetrahedron, 2006 , vol. 62, # 40 p. 9410 - 9416
反应条件
titanium(III) chloride; copper; zinc in tetrahydrofuran
1) reflux, 16 h, 2) r.t., 28 d; Further byproducts given;
参考文献
Laatsch, Hartmut; Talvitie, Antti; Kral, Andreas; Ernst, Bernd-Peter; Noltemeyer, Mathias
Advanced Synthesis and Catalysis, 1996 , vol. 338, # 2 p. 140 - 145
参考文献
Schmid; Seiler
Helvetica Chimica Acta, 1952 , vol. 35, p. 1990,1996
反应条件
1: 97 percent / pyridine / 24 h / 20 °C
2: 96 percent / BF3*Et2O / 0.08 h / 120 °C
View Scheme
参考文献
Nguyen Van, Tuyen; Kesteleyn, Bart; De Kimpe, Norbert
Tetrahedron, 2001 , vol. 57, # 19 p. 4213 - 4219
反应条件
1: 77 percent / SnCl2; aq. HCl / 3 h / Heating
2: 97 percent / pyridine / 24 h / 20 °C
3: 96 percent / BF3*Et2O / 0.08 h / 120 °C
View Scheme
参考文献
Nguyen Van, Tuyen; Kesteleyn, Bart; De Kimpe, Norbert
Tetrahedron, 2001 , vol. 57, # 19 p. 4213 - 4219
反应条件
carbon disulfide; aluminium trichloride
参考文献
Hase; Nishimura
Yakugaku Zasshi, 1955 , vol. 75, p. 203,205,206
Chem.Abstr., 1956 , p. 1712
反应条件
potassium carbonate in acetonitrile
T=20°C; 96 h;
参考文献
Shie, Tien-Lan; Lin, Chi-Hui; Lin, Shih-Lun; Yang, Ding-Yah
European Journal of Organic Chemistry, 2007 , # 29 p. 4831 - 4836
反应条件
potassium carbonate in acetone
24 h; Heating;
参考文献
Nguyen Van, Tuyen; Kesteleyn, Bart; De Kimpe, Norbert
Tetrahedron, 2001 , vol. 57, # 19 p. 4213 - 4219
反应条件
1: 98 percent / K2CO3 / acetone / 24 h / Heating
2: 86 percent / NaBH4 / methanol / 1 h / 20 °C
3: 87 percent / CAN / acetonitrile; H2O / 0.5 h / 20 °C
View Scheme
参考文献
Nguyen Van, Tuyen; Kesteleyn, Bart; De Kimpe, Norbert
Tetrahedron, 2001 , vol. 57, # 19 p. 4213 - 4219
反应条件
1: 60 percent / pyrrolidine / benzene / 48 h / Heating
2: NaBH4 / methanol
3: aq. HCl / methanol / 0.5 h / 65 °C
View Scheme
参考文献
Paradkar, Madhusudan V.; Godbole, Himanshu M.; Ranade, Anup A.; Joseph, Augustine R.
Journal of Chemical Research - Part S, 1998 , # 6 p. 318 - 319
