in hexane; butan-1-ol
byproducts: NaCl; Ar; a soln. of NaOC4H9 in butanol is added dropwise to a suspn. of FeCl3 in hexane; mixt. stirred for 30 min at 20°C, then for 30 min atthe boiling point; NaCl sepd. by centrifugation and extd. (boiling hexane); combined solns. evapd. (vac., 140°C); elem. anal.;
参考文献
Rogova, T. V.; Turova, N. Ya.; Zhdanov, B. V.
Sov. J. Coord. Chem. (Engl. Transl.), 1985 , vol. 11, p. 366 - 372
Koordinatsionnaya Khimiya, 1985 , vol. 11, p. 638 - 644
→
反应条件
in benzene
byproducts: isopropanol; anhydrous conditions; volatilization after evapn.;
参考文献
Shah, A; Singh, J; Singh, A; Mehrotra, R C
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, 1991 , vol. 30, # 12 p. 1018 - 1023
