(9CI)-1,2,3,4-四氢-1,2-二甲基-吡咯并[1,2-a]吡嗪合成路线 （共 4 条）
反应条件
sodium tetrahydroborate in methanol; water
2 h;
参考文献
Jirkovsky, Ivo; Baudy, Reinhardt
Synthesis, 1981 , # 6 p. 481 - 483
反应条件
N-ethyl-N,N-diisopropylamine in acetonitrile
T=20°C; 72 h; Inert atmosphere;
参考文献
Voskressensky; Borisova; Kamalitdinova; Titov; Listratova; Varlamov
Russian Chemical Bulletin, 2010 , vol. 59, # 3 p. 647 - 653
反应条件
1: 71 percent / ethanol / 15 h / Heating
2: 57 percent / NaBH4 / methanol; H2O / 2 h
View Scheme
参考文献
Jirkovsky, Ivo; Baudy, Reinhardt
Synthesis, 1981 , # 6 p. 481 - 483
反应条件
1: 95 percent / POCl3 / 1 h / 20 °C / Heating
2: 71 percent / ethanol / 15 h / Heating
3: 57 percent / NaBH4 / methanol; H2O / 2 h
View Scheme
参考文献
Jirkovsky, Ivo; Baudy, Reinhardt
Synthesis, 1981 , # 6 p. 481 - 483
