4-苄氧基-2-羟基-3-甲基-苯乙酮合成路线 (共 6 条)
反应条件
potassium carbonate; potassium iodide in acetone T=56°C;
参考文献
Gammon, David W.; Hunter, Roger; Wilson, Seanette A.
Tetrahedron, 2005 , vol. 61, # 45 p. 10683 - 10688
反应条件
potassium carbonate in N,N-dimethyl-formamide T=60°C; 16 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 11, # 7 p. 909 - 913
反应条件
1: 78 percent / boron trifluoride-ether complex / 6 h / 70 - 80 °C 2: 81 percent / potassium iodide, potassium carbonate / acetone / 18 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1823 - 1828
反应条件
potassium carbonate in acetone 30 h; Heating;
参考文献
Raphael, Ralph A.; Ravenscroft, Paul
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1823 - 1828
反应条件
1: 82 percent / potassium carbonate / acetone / 30 h / Heating 2: 92 percent / hydrogen / palladium-carbon / ethanol / Ambient temperature View Scheme
参考文献
Raphael, Ralph A.; Ravenscroft, Paul
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1823 - 1828
反应条件
sodium hydride in toluene
T=110°C; 2 h;
参考文献
Gammon, David W.; Hunter, Roger; Wilson, Seanette A.
Tetrahedron, 2005 , vol. 61, # 45 p. 10683 - 10688