Matovic, Nicholas J.; Hayes, Patricia Y.; Penman, Kerry; Lehmann, Reginald P.; De Voss, James J.
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4467 - 4481
1.1: diisobutylaluminium hydride / diethyl ether / 0 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 - -10 °C
2.2: -78 - 20 °C
3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C
3.2: 2 h / 0 °C
View Scheme
参考文献
Matovic, Nicholas J.; Hayes, Patricia Y.; Penman, Kerry; Lehmann, Reginald P.; De Voss, James J.
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4467 - 4481