1-对甲苯磺酰基-3-吡咯烷酮合成路线 （共 11 条）
反应条件
[Au(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)(NTf2)] in toluene T=60°C; 1 h; Molecular sieve;
参考文献
Yeom, Hyun-Suk; So, Eunsu; Shin, Seunghoon
Chemistry - A European Journal, 2011 , vol. 17, # 6 p. 1764 - 1767
反应条件
2-bromopyridine N-oxide; methanesulfonic acid; Et3PAuNTf2 in 1,2-dichloro-ethane T=20°C; 5 h;
参考文献
Shu, Chao; Li, Long; Yu, Yong-Fei; Jiang, Shuang; Ye, Long-Wu
Chemical Communications, 2014 , vol. 50, # 19 p. 2522 - 2525
反应条件
pyridinium chlorochromate in dichloromethane Ambient temperature;
参考文献
Kim, Wan-Joo; Kim, Bong-Jin; Lee, Tae-Suk; Nam, Keun-Soo; Kim, Keun-Jae
Heterocycles, 1995 , vol. 41, # 7 p. 1389 - 1398
反应条件
styrene; copper acetylacetonate in benzene Cyclization; Heating;
参考文献
Wang, Jianbo; Hou, Yihua; Wu, Peng
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 16 p. 2277 - 2280
反应条件
copper acetylacetonate; tri-n-butyl-tin hydride in benzene Cyclization; reduction; 5 h; Heating;
参考文献
Tetrahedron, , vol. 56, # 38 p. 7457 - 7461
反应条件
1: 80.5 percent / NaH / dimethylformamide / 1 h / Ambient temperature 2: 75 percent / NBS, H2O / dimethylsulfoxide 3: 81 percent / (n-Bu)3SnH / tetrahydrofuran / 5 h / Heating 4: 77 percent / PCC / CH2Cl2 / Ambient temperature View Scheme
参考文献
Heterocycles, , vol. 41, # 7 p. 1389 - 1398
反应条件
1: 75 percent / NBS, H2O / dimethylsulfoxide 2: 81 percent / (n-Bu)3SnH / tetrahydrofuran / 5 h / Heating 3: 77 percent / PCC / CH2Cl2 / Ambient temperature View Scheme
参考文献
Heterocycles, , vol. 41, # 7 p. 1389 - 1398
反应条件
1: 81 percent / (n-Bu)3SnH / tetrahydrofuran / 5 h / Heating 2: 77 percent / PCC / CH2Cl2 / Ambient temperature View Scheme
参考文献
Heterocycles, , vol. 41, # 7 p. 1389 - 1398
反应条件
2: rhodium acetate II / CH2Cl2 / 0.08 h / Ambient temperature View Scheme
参考文献
Heterocycles, , vol. 27, # 4 p. 867 - 870
反应条件
1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 0 °C 2: trifluorormethanesulfonic acid / dichloromethane; water; acetonitrile / 1 h / 0 °C 3: [Au(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)(NTf2)] / toluene / 1 h / 60 °C / Molecular sieve View Scheme
参考文献
Chemistry - A European Journal, , vol. 17, # 6 p. 1764 - 1767
