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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
737-76-8
合成路线
（共 11 条）
737-76-8
→
反应条件
18945-38-5
反应条件
adenylate deaminase; dimethyl sulfoxide in phosphate buffer pH=6.5; 2.5 h;
参考文献
Ciuffreda, Pierangela; Loseto, Angela; Alessandrini, Laura; Terraneo, Giancarlo; Santaniello, Enzo
European Journal of Organic Chemistry, 2003 , # 24 p. 4748 - 4751
737-76-8
→
反应条件
14365-44-7
5-氨基腺苷酸
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in N,N-dimethyl acetamide; benzene Heating;
参考文献
Wang, Ting; Lee, Hyun Joo; Tosh, Dilip K.; Kim, Hea Ok; Pal, Shantanu; Choi, Sun; Lee, Yoonji; Moon, Hyung Ryong; Zhao, Long Xuan; Lee, Kang Man; Jeong, Lak Shin
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 16 p. 4456 - 4459
662131-88-6
→
反应条件
737-76-8
反应条件
sodium azide in N,N-dimethyl-formamide T=80°C; 5 h;
参考文献
Ciuffreda, Pierangela; Loseto, Angela; Alessandrini, Laura; Terraneo, Giancarlo; Santaniello, Enzo
European Journal of Organic Chemistry, 2003 , # 24 p. 4748 - 4751
892-48-8
5’-氯-5’-脱氧腺苷
→
反应条件
737-76-8
反应条件
sodium azide in N,N-dimethyl-formamide T=150°C; 1 h; Inert atmosphere;
参考文献
Peterson, Matt A.; Oliveira, Marcelio; Christiansen, Michael A.; Cutler, Christopher E.
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 23 p. 6775 - 6779
34245-48-2
9-[4-(叠氮基甲基)-2,2-二甲基-3a,4,6,6a-四氢呋喃并[3,4-d][1,3]二氧杂环戊烯-6-基]嘌呤-6-胺
→
反应条件
737-76-8
反应条件
trifluoroacetic acid in water T=20°C; 0.333333 h;
参考文献
Comstock, Lindsay R; Rajski, Scott R
Tetrahedron, 2002 , vol. 58, # 30 p. 6019 - 6026
57610-04-5
→
反应条件
737-76-8
反应条件
sodium methylate in methanol T=20°C; 24 h;
参考文献
Wang, Ting; Lee, Hyun Joo; Tosh, Dilip K.; Kim, Hea Ok; Pal, Shantanu; Choi, Sun; Lee, Yoonji; Moon, Hyung Ryong; Zhao, Long Xuan; Lee, Kang Man; Jeong, Lak Shin
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 16 p. 4456 - 4459
68144-26-3
→
反应条件
737-76-8
反应条件
1: aq. trifluoroacetic acid / 1 h / 20 °C 2: sodium methoxide / methanol / 24 h / 20 °C View Scheme
参考文献
Wang, Ting; Lee, Hyun Joo; Tosh, Dilip K.; Kim, Hea Ok; Pal, Shantanu; Choi, Sun; Lee, Yoonji; Moon, Hyung Ryong; Zhao, Long Xuan; Lee, Kang Man; Jeong, Lak Shin
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 16 p. 4456 - 4459
40653-96-1
→
反应条件
737-76-8
反应条件
1: 83 percent / sodium azide / dimethylformamide / 3 h / 60 °C 2: aq. trifluoroacetic acid / 1 h / 20 °C 3: sodium methoxide / methanol / 24 h / 20 °C View Scheme
参考文献
Wang, Ting; Lee, Hyun Joo; Tosh, Dilip K.; Kim, Hea Ok; Pal, Shantanu; Choi, Sun; Lee, Yoonji; Moon, Hyung Ryong; Zhao, Long Xuan; Lee, Kang Man; Jeong, Lak Shin
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 16 p. 4456 - 4459
4546-55-8
N6-苯甲酰基腺苷
→
反应条件
737-76-8
反应条件
1: sulfuric acid / acetone / 0.5 h / 20 °C 2: pyridine / 0.5 h / 20 °C 3: 83 percent / sodium azide / dimethylformamide / 3 h / 60 °C 4: aq. trifluoroacetic acid / 1 h / 20 °C 5: sodium methoxide / methanol / 24 h / 20 °C View Scheme
参考文献
Wang, Ting; Lee, Hyun Joo; Tosh, Dilip K.; Kim, Hea Ok; Pal, Shantanu; Choi, Sun; Lee, Yoonji; Moon, Hyung Ryong; Zhao, Long Xuan; Lee, Kang Man; Jeong, Lak Shin
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 16 p. 4456 - 4459
362-75-4
2',3'-异丙叉腺苷
→
反应条件
737-76-8
反应条件
1: 73.1 percent / diphenylphosphoryl azide; diethyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 36 h / 20 °C 2: CF3CO2H / H2O / 0.33 h / 20 °C View Scheme
参考文献
Comstock, Lindsay R; Rajski, Scott R
Tetrahedron, 2002 , vol. 58, # 30 p. 6019 - 6026
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