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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
73710-48-2
合成路线
（共 8 条）
73710-47-1
→
反应条件
73710-48-2
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
参考文献
Chantrapromma, Kan; McManis, James S.; Ganem, Bruce
Tetrahedron Letters, 1980 , vol. 21, p. 2605 - 2608
112-12-9
2-十一酮
→
反应条件
73710-48-2
反应条件
2: 10 percent NaOH / methanol; H2O / Heating 3: 67 percent / thionyl chloride 4: 82 percent / Na2CO3 / H2O; CH2Cl2 / two-phase system 5: 83 percent / formic acid / Heating 6: 100 percent / H2 / Pd/C / ethyl acetate View Scheme
参考文献
Chantrapromma, Kan; McManis, James S.; Ganem, Bruce
Tetrahedron Letters, 1980 , vol. 21, p. 2605 - 2608
60437-05-0
→
反应条件
73710-48-2
反应条件
1: 10 percent NaOH / methanol; H2O / Heating 2: 67 percent / thionyl chloride 3: 82 percent / Na2CO3 / H2O; CH2Cl2 / two-phase system 4: 83 percent / formic acid / Heating 5: 100 percent / H2 / Pd/C / ethyl acetate View Scheme
参考文献
Chantrapromma, Kan; McManis, James S.; Ganem, Bruce
Tetrahedron Letters, 1980 , vol. 21, p. 2605 - 2608
38972-57-5
→
反应条件
73710-48-2
反应条件
1: 67 percent / thionyl chloride 2: 82 percent / Na2CO3 / H2O; CH2Cl2 / two-phase system 3: 83 percent / formic acid / Heating 4: 100 percent / H2 / Pd/C / ethyl acetate View Scheme
参考文献
Chantrapromma, Kan; McManis, James S.; Ganem, Bruce
Tetrahedron Letters, 1980 , vol. 21, p. 2605 - 2608
76524-64-6
→
反应条件
73710-48-2
反应条件
1: 82 percent / Na2CO3 / H2O; CH2Cl2 / two-phase system 2: 83 percent / formic acid / Heating 3: 100 percent / H2 / Pd/C / ethyl acetate View Scheme
参考文献
Chantrapromma, Kan; McManis, James S.; Ganem, Bruce
Tetrahedron Letters, 1980 , vol. 21, p. 2605 - 2608
76524-66-8
→
反应条件
73710-48-2
反应条件
1: 82 percent / Na2CO3 / H2O; CH2Cl2 / two-phase system 2: 83 percent / formic acid / Heating 3: 100 percent / H2 / Pd/C / ethyl acetate View Scheme
参考文献
Chantrapromma, Kan; McManis, James S.; Ganem, Bruce
Tetrahedron Letters, 1980 , vol. 21, p. 2605 - 2608
76524-63-5
→
反应条件
73710-48-2
反应条件
1: 57 percent / LiAlH4 2: 82 percent / Na2CO3 / H2O; CH2Cl2 / two-phase system 3: 83 percent / formic acid / Heating 4: 100 percent / H2 / Pd/C / ethyl acetate View Scheme
参考文献
Chantrapromma, Kan; McManis, James S.; Ganem, Bruce
Tetrahedron Letters, 1980 , vol. 21, p. 2605 - 2608
76524-67-9
→
反应条件
73710-48-2
反应条件
1: 83 percent / formic acid / Heating 2: 100 percent / H2 / Pd/C / ethyl acetate View Scheme
参考文献
Chantrapromma, Kan; McManis, James S.; Ganem, Bruce
Tetrahedron Letters, 1980 , vol. 21, p. 2605 - 2608
