苯并[1,2,5]噻二唑-4-磺酰氯合成路线 (共 5 条)
反应条件
sulfuryl dichloride in acetic acid T=55 - 65°C; 0.333333 h;
参考文献
Belen'kaya, I. A.; Shulla, T. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 11 p. 1303 - 1307
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 11 p. 1555 - 1558
反应条件
chlorosulfonic acid T=130 - 135°C; 6 h;
参考文献
Dorogov, Mikhail V.; Filimonov, Sergey I.; Kobylinsky, Dmitry B.; Ivanovsky, Sergey A.; Korikov, Pavel V.; Soloviev, Mikhail Y.; Khahina, Maria Y.; Shalygina, Elena E.; Kravchenko, Dmitry V.; Ivachtchenko, Alexandre V.
Synthesis, 2004 , # 18 p. 2999 - 3004
反应条件
water; chlorine in acetic acid 3 h;
参考文献
Belen'kaya, I. A.; Shulla, T. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 11 p. 1303 - 1307
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 11 p. 1555 - 1558
反应条件
sodium hydroxide; sodium sulfite
参考文献
Pesin,V.G. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, # 4 p. 1267 - 1272,1265 - 1269
反应条件
ammonia in dichloromethane
T=-78°C; 4 h;
参考文献
Chern, Ji-Wang; Leu, Yu-Ling; Wang, Shan-Shue; Jou, Ruwen; Lee, Chin-Fen; Tsou, Pei-Chie; Hsu, Shih-Chung; Liaw, Yen-Chywan; Lin, Hua-Mei
Journal of Medicinal Chemistry, 1997 , vol. 40, # 14 p. 2276 - 2286