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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-(苯基氨基)丁腈
合成路线
（共 14 条）
73747-25-8
4-(苯基氨基)丁腈
→
反应条件
148494-90-0
1-苯基哌啶-3-酮
反应条件
1: K2CO3 2: aq.-ethanolic HCl 3: sodium ethylate; toluene / anschliessenden Erwaermen mit konz. Salzsaeure View Scheme
参考文献
Leonard et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 3727,3730
110-61-2
丁二腈
+
74497-02-2
→
反应条件
73747-25-8
4-(苯基氨基)丁腈
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; 27 h;
参考文献
Ikawa, Takashi; Fujita, Yuki; Mizusaki, Tomoteru; Betsuin, Sae; Takamatsu, Haruki; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 2 p. 293 - 304
1765-93-1
4-氟苯硼酸
+
112933-58-1
→
反应条件
73747-25-8
4-(苯基氨基)丁腈
+
75343-38-3
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
32316-92-0
2-萘硼酸
+
112933-58-1
→
反应条件
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
128796-39-4
4-三氟甲基苯硼酸
+
112933-58-1
→
反应条件
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
112933-58-1
+
139301-27-2
4-三氟甲氧基苯硼酸
→
反应条件
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
112933-58-1
+
98-80-6
苯硼酸
→
反应条件
73747-25-8
4-(苯基氨基)丁腈
+
24398-61-6
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
55552-70-0
3-呋喃硼酸
+
112933-58-1
→
反应条件
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
112933-58-1
+
182163-96-8
3,4,5-三甲氧基苯硼酸
→
反应条件
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
628-20-6
4-氯丁腈
+
74497-02-2
→
反应条件
73747-25-8
4-(苯基氨基)丁腈
反应条件
sodium hydrogencarbonate in N,N-dimethyl-formamide 16 h; Heatingwater bath;
参考文献
Korbonits, Dezsoe; Horvath, Karoly; Goenczi, Csaba; Tamas, Jozsef
Acta Chimica Hungarica, 1984 , vol. 117, # 3 p. 239 - 246
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