1-吲哚-1-基丙-1-酮合成路线 (共 5 条)
反应条件
copper(I) thiophene-2-carboxylate; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene
T=110°C; 24 h; Inert atmosphere;
参考文献
Hodgkinson, Roy C.; Schulz, Jurgen; Willis, Michael C.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 3 p. 432 - 434
反应条件
copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene
T=110°C; 24 h; Inert atmosphere;
参考文献
Hodgkinson, Roy C.; Schulz, Jurgen; Willis, Michael C.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 3 p. 432 - 434
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
72 h; Inert atmosphere;
参考文献
Trost, Barry M.; Michaelis, David J.; Charpentier, Julie; Xu, Jiayi
Angewandte Chemie - International Edition, 2012 , vol. 51, # 1 p. 204 - 208
反应条件
lithium diisopropyl amide
1) diglyme, -78 deg C, 30 min, 2) r.t., 1 h; Yield given. Multistep reaction;
参考文献
Ito; Kobayashi; Seko; Saegusa
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 73 - 84
参考文献
Horiie
Memoirs of the Institute of Scientific and Industrial Research, Osaka University, 1950 , vol. 7, p. 143,145
Chem.Abstr., 1951 , p. 9030