NH3 in ammonia
NH3 (liquid); slow addn. of (CH3)3SiCl to liq. NH3 at about -75°C;;
参考文献
Sauer, R. O.; Hasek, R. H.
Journal of the American Chemical Society, 1946 , vol. 68, p. 241 - 244
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Gmelin Handbook: Si: MVol.C, 112, page 314 - 316
NaNH2 in tetrahydrofuran
under N2, dropwise addn. of boron-compd. in THF to a -78°C cold soln. of NaNH2 in THF, warmed to room temp.; all volatiles pumped off, treated with petroleum ether;
参考文献
Schmid, Guenter; Polk, Michael; Boese, Roland
Inorganic Chemistry, 1990 , vol. 29, p. 4421 - 4429
