2-羟基-3-萘-2-基苯并吡喃-4-酮合成路线 (共 2 条)
反应条件
lithium hydroxide; tri-tert-butyl phosphine; palladium diacetate in ethylene glycol dimethyl ether; water
T=25°C; Suzuki coupling reaction; 14 h;
参考文献
Zhu, Qiang; Wu, Jie; Fathi, Reza; Yang, Zhen
Organic Letters, 2002 , vol. 4, # 19 p. 3333 - 3336
反应条件
1.1: Na2CO3 / H2O / 0.5 h / 20 °C
1.2: Na2CO3 / H2O / 2 h / 20 °C
2.1: 80 percent / LiOH*H2O; P(t-Bu)3 / Pd(OAc)2 / 1,2-dimethoxy-ethane; H2O / 14 h / 25 °C
View Scheme
参考文献
Zhu, Qiang; Wu, Jie; Fathi, Reza; Yang, Zhen
Organic Letters, 2002 , vol. 4, # 19 p. 3333 - 3336