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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
73796-06-2
合成路线
（共 14 条）
112152-12-2
→
反应条件
73796-06-2
+
75446-85-4
反应条件
hydrogen; palladium on activated charcoal in methanol
参考文献
Somei, Masanori; Karasawa, Yoshio; Kaneko, Chikara
Chemistry Letters, 1980 , p. 813 - 816
42792-95-0
→
反应条件
73796-06-2
反应条件
1: 1.) aq. TiCl3; 2.) pyridine 2: 30percent aq. NaOH-MeOH / 4 h / Heating 3: 8 percent / active MnO2, NaOH 4: 64 percent / hydrogen / 5percent Pd-C / methanol View Scheme
参考文献
Somei, Masanori; Karasawa, Yoshio; Kaneko, Chikara
Chemistry Letters, 1980 , p. 813 - 816
75446-71-8
→
反应条件
73796-06-2
反应条件
1: 30percent aq. NaOH-MeOH / 4 h / Heating 2: 8 percent / active MnO2, NaOH 3: 64 percent / hydrogen / 5percent Pd-C / methanol View Scheme
参考文献
Somei, Masanori; Karasawa, Yoshio; Kaneko, Chikara
Chemistry Letters, 1980 , p. 813 - 816
3468-22-2
→
反应条件
73796-06-2
反应条件
1: 8 percent / active MnO2, NaOH 2: 64 percent / hydrogen / 5percent Pd-C / methanol View Scheme
参考文献
Somei, Masanori; Karasawa, Yoshio; Kaneko, Chikara
Chemistry Letters, 1980 , p. 813 - 816
1074-86-8
4-吲哚甲醛
→
反应条件
73796-06-2
反应条件
1: 98 percent / 3.3percent aq. NaOH 2: 64 percent / hydrogen / 5percent Pd-C / methanol View Scheme
参考文献
Somei, Masanori; Karasawa, Yoshio; Kaneko, Chikara
Chemistry Letters, 1980 , p. 813 - 816
1074-85-7
吲哚-4-甲醇
→
反应条件
73796-06-2
反应条件
1: 73 percent / active MnO2 / acetone 2: 98 percent / 3.3percent aq. NaOH 3: 64 percent / hydrogen / 5percent Pd-C / methanol View Scheme
参考文献
Somei, Masanori; Karasawa, Yoshio; Kaneko, Chikara
Chemistry Letters, 1980 , p. 813 - 816
75446-86-5
→
反应条件
73796-06-2
反应条件
1: 91 percent / Jones oxidation 2: 91 percent / Heating 3: 63 percent / hydrogen / 5percent Pd-C 4: 77 percent / 6N-HCl / methanol 5: 20 percent / active MnO2 / CH2Cl2 View Scheme
参考文献
Somei, Masanori; Karasawa, Yoshio; Kaneko, Chikara
Chemistry Letters, 1980 , p. 813 - 816
74068-99-8
→
反应条件
73796-06-2
反应条件
1: 1.) AC2O; 2.) 2N NaOH / 1.) 3.5 h, reflux; 2.) MeOH, 1 min, reflux 2: 73 percent / active MnO2 / acetone 3: 98 percent / 3.3percent aq. NaOH 4: 64 percent / hydrogen / 5percent Pd-C / methanol View Scheme
参考文献
Somei, Masanori; Karasawa, Yoshio; Kaneko, Chikara
Chemistry Letters, 1980 , p. 813 - 816
75446-77-4
→
反应条件
73796-06-2
反应条件
1: 1.) AC2O; 2.) 2N NaOH / 1.) 3.5 h, reflux; 2.) MeOH, 1 min, reflux 2: 73 percent / active MnO2 / acetone 3: 98 percent / 3.3percent aq. NaOH 4: 64 percent / hydrogen / 5percent Pd-C / methanol View Scheme
参考文献
Somei, Masanori; Karasawa, Yoshio; Kaneko, Chikara
Chemistry Letters, 1980 , p. 813 - 816
75446-87-6
→
反应条件
73796-06-2
反应条件
1: 91 percent / Heating 2: 63 percent / hydrogen / 5percent Pd-C 3: 77 percent / 6N-HCl / methanol 4: 20 percent / active MnO2 / CH2Cl2 View Scheme
参考文献
Somei, Masanori; Karasawa, Yoshio; Kaneko, Chikara
Chemistry Letters, 1980 , p. 813 - 816
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