1-甲氧基-4-苯基乙炔苯合成路线 （共 169 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetra-(n-butyl)ammonium iodide; diethylamine in acetonitrile
T=20°C; Sonogashira coupling; 1 h; Inert atmosphere;
参考文献
Panda, Biswajit; Sarkar, Tarun K.
Chemical Communications, 2010 , vol. 46, # 18 p. 3131 - 3133
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in tetrahydrofuran; acetonitrile
T=60°C; Sonogashira coupling; 2 h; Inert atmosphere;
参考文献
Man, Wing Y.; Bock, Soeren; Zaitseva, Natasha N.; Bruce, Michael I.; Low, Paul J.
Journal of Organometallic Chemistry, 2011 , vol. 696, # 10 p. 2172 - 2176
反应条件
2,6-dimethylpyridine; oxygen; copper(I) bromide in methanol
T=45°C; Sonogashira coupling; P=760.051 Torr; 16 h;
参考文献
Yasukawa, Tomohiro; Miyamura, Hiroyuki; Kobayashi, Sh
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 18 p. 6208 - 6210
反应条件
diisopropyl-carbodiimide in dichloromethane
T=25°C; 24 h; Inert atmosphere;
参考文献
Wardrop, Duncan J.; Komenda, John P.
Organic Letters, 2012 , vol. 14, # 6 p. 1548 - 1551
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene in ethylene glycol dimethyl ether; n-heptane
T=20°C; 5 h;
参考文献
Wang, Baomin; Bonin, Martine; Micouin, Laurent
Organic Letters, 2004 , vol. 6, # 20 p. 3481 - 3484
反应条件
potassium phosphate; triphenylphosphine; palladium diacetate in dimethyl sulfoxide
T=80°C; 24 h;
参考文献
Shirakawa, Eiji; Kitabata, Takaaki; Otsuka, Hidehito; Tsuchimoto, Teruhisa
Tetrahedron, 2005 , vol. 61, # 41 p. 9878 - 9885
反应条件
1: benzene With iodine; silver trifluoromethanesulfonate in 1,2-dichloro-ethane
T=20°C; 0.0833333 h;
2: 4-ethynyl-1-methoxy-benzene With piperidine; bis-triphenylphosphine-palladium(II) chloride in 1,2-dichloro-ethane
T=70°C; 3 h;
参考文献
Wan, Shun; Wang, Sunewang R.; Lu, Wenjun
Journal of Organic Chemistry, 2006 , vol. 71, # 11 p. 4349 - 4352
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=90°C; 2 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Jadhav, Deepak N.; Dasgupta, Priyabrata
Organic Letters, 2010 , vol. 12, # 9 p. 2048 - 2051
反应条件
1: 4-methoxy-aniline With tert.-butylnitrite; boron trifluoride diethyl etherate in tetrahydrofuran
T=0°C;
2: phenylacetylene With 2,6-di-tert-butyl-4-methylpyridine; gold(I) chloride; palladium dichloride; SIDip*HCl in tetrahydrofuran; acetonitrile
T=20°C; Sonogashira coupling;
参考文献
Panda, Biswajit; Sarkar, Tarun K.
Chemical Communications, 2010 , vol. 46, # 18 p. 3131 - 3133
反应条件
triphenylphosphine; bis(acetylacetonato) palladium in tetrahydrofuran
T=40°C; 4 h;
参考文献
Dzhemilev, U. M.; Saraev, R. A.; Vyrypaev, E. M.; Ibragimov, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 9 p. 1888 - 1892
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 9 p. 2037 - 2041
