Collins, Michael P.; Drew, Michael G. B.; Mann, John; Finch, Harry
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 23 p. 3211 - 3218
1: 68 percent / H2 / 10percent Pd-C / benzene / 6.5 h / 2585.7 Torr
2: 87 percent / DIBAL / CH2Cl2; diethyl ether / 4 h / -78 °C
3: 68 percent / MnO2 / CH2Cl2 / Ambient temperature
4: 90 percent / glacial HOAc / 3.5 h / 0 °C
View Scheme
参考文献
Collins, Michael P.; Drew, Michael G. B.; Mann, John; Finch, Harry
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 23 p. 3211 - 3218
1: 68 percent / H2 / 10percent Pd-C / benzene / 6.5 h / 2585.7 Torr
2: 87 percent / DIBAL / CH2Cl2; diethyl ether / 4 h / -78 °C
3: 68 percent / MnO2 / CH2Cl2 / Ambient temperature
4: 90 percent / glacial HOAc / 3.5 h / 0 °C
5: MeI / propan-2-ol; H2O / Ambient temperature
View Scheme
参考文献
Collins, Michael P.; Drew, Michael G. B.; Mann, John; Finch, Harry
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 23 p. 3211 - 3218