3,4'-二甲基-1,1'-联苯合成路线 （共 62 条）
反应条件
trifluorormethanesulfonic acid
T=20°C; KineticsProduct distribution; Further Variations:TemperaturesSolventsacid/substrate ratio;
参考文献
Sherman, S. Christopher; Iretskii, Alexei V.; White, Mark G.; Gumienny, Charles; Tolbert, Laren M.; Schiraldi, David A.
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 2034 - 2041
反应条件
trifluorormethanesulfonic acid
T=20°C; KineticsProduct distribution; Further Variations:TemperaturesSolventsacid/substrate ratio;
参考文献
Sherman, S. Christopher; Iretskii, Alexei V.; White, Mark G.; Gumienny, Charles; Tolbert, Laren M.; Schiraldi, David A.
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 2034 - 2041
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl in toluene
T=120°C; 6 h; Mechanism;
参考文献
Tseng, Chia-Kai; Lee, Chi-Rung; Tseng, Mei-Chun; Han, Chien-Chung; Shyu, Shin-Guang
Dalton Transactions, 2014 , vol. 43, # 19 p. 7020 - 7027
反应条件
(i) polyphosphoric acid, (ii) sulfur; Multistep reaction;
参考文献
Colonge,J.; Brunie,J.-C.
Bulletin de la Societe Chimique de France, 1963 , p. 42 - 46
反应条件
(i) H2, Raney-Ni, (ii) NaNO2, aq. HCl, (iii) H3PO2; Multistep reaction;
参考文献
Harrison,C.R. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 1769 - 1771
反应条件
in toluene
was heated at 70°C for 2h; was filtered; filtrate was concentrated under reduced pressure; was diluted with hexane; GLC;
参考文献
Fuchita, Yoshio; Hiraki, Katsuma; Kamogawa, Yasuko; Suenaga, Miho; Tohgoh, Kazutaka; Fujiwara, Yuzo
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 4 p. 1081 - 1085
参考文献
Epelberg; Lowy
Journal of the American Chemical Society, 1941 , vol. 63, p. 101
反应条件
in toluene
T=120°C; 6 h; Mechanism;
参考文献
Tseng, Chia-Kai; Lee, Chi-Rung; Tseng, Mei-Chun; Han, Chien-Chung; Shyu, Shin-Guang
Dalton Transactions, 2014 , vol. 43, # 19 p. 7020 - 7027
反应条件
in acetonitrile
Irradiationalso in acetone; also with triflate; Product distribution;
参考文献
Dektar, John L.; Hacker, Nigel P.
Journal of Organic Chemistry, 1990 , vol. 55, # 2 p. 639 - 647
反应条件
palladium diacetate
T=60 - 70°C; selectivity in the oxidative coupling; influence of Tl(CF3COO)3; partial rate factors; Product distribution;
参考文献
Deiko, S. A.; Ryabov, A. D.; Yatsimirskii, A. K.; Berezin, I. B.
Doklady Chemistry, 1982 , vol. 266, p. 356 - 359
Dokl. Akad. Nauk SSSR Ser. Khim., 1982 , vol. 266, # 4 p. 874 - 878
