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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
73845-05-3
合成路线
（共 11 条）
73845-05-3
+
16640-68-9
(三苯基膦)乙腈
→
反应条件
1885-38-7
肉桂腈
+
24840-05-9
反应条件
in acetonitrile T=25°C; 24 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
73845-05-3
+
20913-05-7
→
反应条件
614-47-1
反式-查耳酮
反应条件
in dimethyl sulfoxide T=100°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
73845-05-3
+
69052-20-6
→
反应条件
886-65-7
反,反-1,4-二苯基-1,3-丁二烯
反应条件
1: E-cinnamyltriphenylphosphonium chloride in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: N-(Phenylmethylene)methanesulphonamide in tetrahydrofuran; hexane T=-78 - 20°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Dong, De-Jun; Li, Hai-Hua; Tian, Shi-Kai
Journal of the American Chemical Society, 2010 , vol. 132, # 14 p. 5018 - 5020
73845-05-3
+
69052-20-6
→
反应条件
886-65-7
反,反-1,4-二苯基-1,3-丁二烯
反应条件
1: E-cinnamyltriphenylphosphonium chloride in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: N-(Phenylmethylene)methanesulphonamide in tetrahydrofuran; hexane T=-78 - 20°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Dong, De-Jun; Li, Hai-Hua; Tian, Shi-Kai
Journal of the American Chemical Society, 2010 , vol. 132, # 14 p. 5018 - 5020
73845-05-3
+
1449-46-3
三苯基苄基溴化膦
→
反应条件
645-49-8
顺式-二苯乙烯
+
103-30-0
反式-1,2-二苯乙烯
反应条件
1: triphenylbenzyl-phosphonium bromide in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: N-(Phenylmethylene)methanesulphonamide in tetrahydrofuran; hexane T=-78 - 20°C; 12 h; Inert atmosphere;
参考文献
Dong, De-Jun; Li, Hai-Hua; Tian, Shi-Kai
Journal of the American Chemical Society, 2010 , vol. 132, # 14 p. 5018 - 5020
73845-05-3
+
16640-68-9
(三苯基膦)乙腈
→
反应条件
1885-38-7
肉桂腈
+
24840-05-9
反应条件
in acetonitrile T=25°C; 24 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
73845-05-3
+
1099-45-2
乙氧甲酰基亚甲基三苯基膦
→
反应条件
4192-77-2
反式-肉桂酸乙酯
反应条件
in para-xylene T=140°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
73845-05-3
+
1099-45-2
乙氧甲酰基亚甲基三苯基膦
→
反应条件
4610-69-9
顺式-乙基肉桂酸酯
+
4192-77-2
反式-肉桂酸乙酯
反应条件
in dichloromethane T=25°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
91-63-4
2-甲基喹啉
+
73845-05-3
→
反应条件
38101-69-8
反应条件
in toluene T=120°C; 12 h; Inert atmosphere; optical yield given as percent de;
参考文献
Yan, Yizhe; Xu, Kun; Fang, Yang; Wang, Zhiyong
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6849 - 6855
73845-05-3
→
反应条件
3989-45-5
反应条件
diethylzinc in hexane; toluene T=20°C; 1 h;
参考文献
Gao, Feifeng; Deng, Minzhi; Qian, Changtao
Tetrahedron, 2005 , vol. 61, # 52 p. 12238 - 12243
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