2’,3’,5’-三乙酰腺苷合成路线 (共 40 条)
反应条件
pyridine 6 h; Ambient temperature;
参考文献
Reese, Colin B.; Shek, Louise H. K.; Zhao, Zhengyun
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 24 p. 3077 - 3084
反应条件
ammonia; oxygen; ozone in dichloromethane T=0°C; 0.0833333 h;
参考文献
Saladino, Raffaele; Mincione, Enrico; Crestini, Claudia; Mezzetti, Maurizio
Tetrahedron, 1996 , vol. 52, # 19 p. 6759 - 6780
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile 18 h; Ambient temperature;
参考文献
Himmelsbach, Frank; Schulz, Bernd S.; Trichtinger, Thomas; Charubala, Ramamurthy; Pfleiderer, Wolfgang
Tetrahedron, 1984 , vol. 40, # 1 p. 59 - 72
反应条件
4-(N,N-dimethlyamino)pyridine in pyridine T=20°C; 24 h; Cooling with ice;
参考文献
Wolf, Joern; Dombos, Valeska; Appel, Bettina; Mueller, Sabine
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 5 p. 899 - 907
反应条件
potassium permanganate in water; acetic acid T=40°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 22, # 33 p. 3205 - 3208
反应条件
in methanol T=105°C; 3 h;
参考文献
Nowak, Ireneusz; Conda-Sheridan, Martin; Robins, Morris J.
Journal of Organic Chemistry, 2005 , vol. 70, # 18 p. 7455 - 7458
反应条件
potassium permanganate in water; acetic acid 0.5 h; Ambient temperature;
参考文献
Kato, Tetsuo; Ogawa, Shuichi; Ito, Isoo
Tetrahedron Letters, 1981 , vol. 22, # 33 p. 3205 - 3208
反应条件
1: 6-aminopurine With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane 2.5 h; Heating; 2: (2R,3R,4R,5S)-4,5-bis(acetyloxy)-2-[(acetyloxy)methyl]tetrahydro-3-furanyl acetate With trimethylsilyl trifluoromethanesulfonate in acetonitrile T=20°C; 1.33333 h;
参考文献
Tetrahedron, , vol. 62, # 43 p. 10123 - 10129
反应条件
potassium permanganate in water; acetic acid T=40°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 22, # 33 p. 3205 - 3208
反应条件
toluene-4-sulfonic acid in chlorobenzene T=150°C; 2.5 h;
参考文献
Tetrahedron, , vol. 62, # 43 p. 10123 - 10129