2’,3’,5’-三乙酰腺苷合成路线 （共 40 条）
反应条件
1: 42.5 percent / KMnO4 / acetic acid; H2O / 0.5 h / Ambient temperature 2: 83.2 percent / KMnO4 / acetic acid; H2O / 0.5 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 22, # 33 p. 3205 - 3208
反应条件
1: 96 percent / dioxane / 0.5 h / Ambient temperature 2: 0.01 M HCl / aq. ethanol / 96 h / Ambient temperature View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 30, # 5 p. 1181 - 1189
反应条件
1: hydrazine hydrate / ethanol / 24 h / |Reflux 2: copper(II) sulfate; water; oxygen / 6 h / 80 °C / |Green chemistry View Scheme
参考文献
Green Chemistry, , vol. 16, # 3 p. 1077 - 1081
反应条件
pyridine Erwaermen des Reaktionsprodukts mit wss.Essigsaeure;
参考文献
Journal of the Chemical Society, , p. 1442,1445
Journal of the Chemical Society, , p. 1546,1548
反应条件
1: 88 percent / pyridine / 20 h / 100 °C 2: 94 percent / dimethylformamide / 0.25 h / Ambient temperature View Scheme
参考文献
Nair, Vasu; Young, David A.
Synthesis, 1986 , # 6 p. 450 - 453
反应条件
disodium hydrogenphosphate; bromine in 1,4-dioxane 0.25 h; Ambient temperature;
参考文献
Maki, Yoshifumi; Makino, Toru; Hirota, Kosaku; Sako, Magoichi
Heterocycles, 1993 , vol. 35, # 1 p. 325 - 337
反应条件
tert-Butyl thionitrate; copper dichloride in acetonitrile T=25°C; 24 h;
参考文献
Kim, Yong Hae
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 74, # 1-4 p. 249 - 260
反应条件
1: 46 percent / tert-butyl nitrite; SbI3 / various solvent(s); tetrahydrofuran / 0.17 h / 60 °C 2: 76 percent / NH3 / methanol / -5 - 0 °C View Scheme
参考文献
Francom, Paula; Janeba, Zlatko; Shibuya, Susumu; Robins, Morris J.
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6788 - 6796
参考文献
Saladino, Raffaele; Mincione, Enrico; Crestini, Claudia; Mezzetti, Maurizio
Tetrahedron, 1996 , vol. 52, # 19 p. 6759 - 6780
反应条件
fluorine in chloroform 1 h; Ambient temperature;
参考文献
Barrio, Jorge R.; Namavari, Mohammad; Phelps, Michael E.; Satyamurthy, Nagichettiar
Journal of the American Chemical Society, 1996 , vol. 118, # 43 p. 10408 - 10411
