2,3-双(三氟甲基)吡唑并[1,5-a]吡啶合成路线 (共 3 条)
反应条件
potassium carbonate in tetrahydrofuran
T=20°C; 24 h;
参考文献
BIOLIPOX AB
Patent: WO2007/51981 A1, 2007 ;
Location in patent: Page/Page column 54 ;
反应条件
potassium carbonate in dichloromethane
1.) -196 deg C to room temperature, 2.) room temperature, 5 d;
参考文献
Banks, Ronald E.; Hitchen, Stephen M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 7 p. 1593 - 1600
反应条件
potassium carbonate in dichloromethane
1.) -196 deg C to room temperature, 2.) room temperature, 5 d;
参考文献
Banks, Ronald E.; Hitchen, Stephen M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 7 p. 1593 - 1600