反应条件
1: triethylamine / tetrahydrofuran / 3 h / 0 °C / |Inert atmosphere
2: phosphorus pentachloride / dichloromethane / 24 h / |Inert atmosphere; |Reflux
3: sodium t-butanolate; palladium diacetate; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine / toluene / 18 h / 100 °C / |Inert atmosphere
View Scheme
参考文献
Sadig, Jessie E. R.; Foster, Radleigh; Willis, Michael C.; Wakenhut, Florian
Journal of Organic Chemistry, 2012 , vol. 77, # 21 p. 9473 - 9486,14