6-溴-3-甲基-1,3-苯并噻唑-2(3H)-亚胺合成路线 (共 6 条)
反应条件
in ethanol
15 h; Heating;
参考文献
Lin; Kasina
Journal of Heterocyclic Chemistry, 1981 , vol. 18, # 4 p. 759 - 761
反应条件
1: 92 percent / bromine / acetic acid / 0.5 h / 10 °C
2: 63 percent / ethanol / 15 h / Heating
View Scheme
参考文献
Lin; Kasina
Journal of Heterocyclic Chemistry, 1981 , vol. 18, # 4 p. 759 - 761
参考文献
Hunter et al.
Journal of the Chemical Society, 1959 , p. 784,787
参考文献
Hunter; Jones
Journal of the Chemical Society, 1930 , p. 2190,2209
反应条件
1: 50percent aq. KOH / Heating
2: 82 percent / sodium carbonate / ethanol / 10 h / Heating
View Scheme
参考文献
Lin; Kasina
Journal of Heterocyclic Chemistry, 1981 , vol. 18, # 4 p. 759 - 761
反应条件
1: 50percent aq. KOH / Heating
2: 82 percent / sodium carbonate / ethanol / 10 h / Heating
3: 85 percent / copper powder, cuprous iodide, sodium carbonate / dimethylformamide / 12 h / Heating
View Scheme
参考文献
Lin; Kasina
Journal of Heterocyclic Chemistry, 1981 , vol. 18, # 4 p. 759 - 761