(R)-(-)-2-溴-1-苯乙醇合成路线 (共 8 条)
反应条件
alkaline H2O2; lithium triethylborohydride 1.) THF, RT, overnight; Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, Herbert C.; Pai, G. Ganesh
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1384 - 1394
反应条件
lithium triethylborohydride in tetrahydrofuran
参考文献
Brown, Herbert C; Pai, Ganesh G.
Journal of Organic Chemistry, 1983 , vol. 48, # 10 p. 1784 - 1786
反应条件
alkaline H2O2; lithium triethylborohydride 1.) THF, RT, overnight; Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, Herbert C.; Pai, G. Ganesh
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1384 - 1394
反应条件
Alkaline Title compound not separated from byproducts;
参考文献
Soai, Kenso; Yamanoi, Takashi; Hikima, Hitoshi
Journal of Organometallic Chemistry, 1985 , vol. 290, p. C23 - C26
反应条件
potassium hydroxide in chloroform; water optical yield given as percent ee;
参考文献
Wu, Guofeng; Zhu, Jinlong; Ding, Zhenhua; Shen, Zongxuan; Zhang, Yawen
Tetrahedron Letters, 2009 , vol. 50, # 4 p. 427 - 429
反应条件
Alkaline Title compound not separated from byproducts;
参考文献
Soai, Kenso; Yamanoi, Takashi; Hikima, Hitoshi
Journal of Organometallic Chemistry, 1985 , vol. 290, p. C23 - C26
反应条件
ammonia in water T=20°C; 2 h;
参考文献
Yu, Feng; Zhou, Ji-Ning; Zhang, Xi-Chang; Sui, Yao-Zong; Wu, Fei-Fei; Xie, Lin-Jie; S. C. Chan, Albert; Wu, Jing
Chemistry - A European Journal, 2011 , vol. 17, # 50 p. 14234 - 14240
反应条件
sodium azide in N,N-dimethyl-formamide
T=80°C; 8 h;
参考文献
Yu, Feng; Zhou, Ji-Ning; Zhang, Xi-Chang; Sui, Yao-Zong; Wu, Fei-Fei; Xie, Lin-Jie; S. C. Chan, Albert; Wu, Jing
Chemistry - A European Journal, 2011 , vol. 17, # 50 p. 14234 - 14240