2-甲酰基-4-噻唑羧酸乙酯合成路线 （共 7 条）
反应条件
hydrogenchloride in acetone 0.75 h; Heating;
参考文献
Inami; Shiba
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 1 p. 352 - 360
反应条件
1: 58 percent / ethanol / 1 h / Heating 2: 92 percent / aq. HCl / acetone / 1 h / Heating View Scheme
参考文献
Organic Letters, , vol. 6, # 19 p. 3401 - 3404
反应条件
1: With selenium(IV) oxide; acetic acid 12 h; RefluxInert atmosphere; 2: With sodium hydrogencarbonate in water
参考文献
Journal of Organic Chemistry, , vol. 74, # 15 p. 5750 - 5753
反应条件
selenium(IV) oxide in acetic acid 12 h; Reflux;
参考文献
Aulakh, Virender S.; Ciufolini, Marco A.
Journal of the American Chemical Society, 2011 , vol. 133, # 15 p. 5900 - 5904
反应条件
1: trichloromonobromomethane; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1.17 h / 0 °C 2: hydrogenchloride / water; acetone / 1 h / Reflux View Scheme
参考文献
Synthetic Communications, , vol. 42, # 14 p. 2098 - 2109
反应条件
1: 12-molybdophosphoric acid HPMo / ethanol / 3 h / 120 °C / Microwave irradiation 2: trichloromonobromomethane; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1.17 h / 0 °C 3: hydrogenchloride / water; acetone / 1 h / Reflux View Scheme
参考文献
Synthetic Communications, , vol. 42, # 14 p. 2098 - 2109
反应条件
1: tetrahydrofuran; toluene / 12 h / 0 °C 2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere View Scheme
参考文献
Fache; Cros; Piva; Lefebvre
Synthetic Communications, 2012 , vol. 42, # 14 p. 2098 - 2109
