2,4,5,7-四甲基菲合成路线 （共 11 条）
反应条件
chromic acid in acetic acid
参考文献
Ho, Tong-Ing; Chang, Cheu-Ming; Wang, Sen Ren; Cheng, Cheu Pyeng
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 123 - 128
反应条件
osmium(VIII) oxide in pyridine 96 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Mervic, Miljenko; Ghera, Eugene
Journal of Organic Chemistry, 1980 , vol. 45, # 23 p. 4720 - 4725
反应条件
iodine in cyclohexane
24 h; Irradiation;
参考文献
Ho, Tong-Ing; Shu, Cheng-Shein; Yeh, Ming-Kuo; Chen, Fa-Ching
Synthesis, 1987 , # 9 p. 795 - 797
反应条件
rhodium on alumina
T=302 - 306°C;
参考文献
Karnes,H.A. et al.
Journal of the American Chemical Society, 1965 , vol. 87, # 24 p. 5554 - 5558
反应条件
1: Me3N, MeSO2Cl
2: NaNH2 / liquid ammonia
View Scheme
参考文献
Newman,M.S.; Lilje,K.C.
Journal of Organic Chemistry, 1979 , vol. 44, # 26 p. 4944 - 4946
反应条件
1: (i) aq. HCl, NaNO2, (ii) NH2OH*H2SO4, CuSO4, aq. NH3, aq. NaOH, (iii) Zn, aq. NaOH
2: H2SO4
3: LiAlH4
4: PBr3
5: PhLi
6: Rh-Al2O3 / 302 - 306 °C
View Scheme
参考文献
Karnes,H.A. et al.
Journal of the American Chemical Society, 1965 , vol. 87, # 24 p. 5554 - 5558
反应条件
1: aq. H2O2, aq. NaOH
2: (i) aq. HCl, NaNO2, (ii) NH2OH*H2SO4, CuSO4, aq. NH3, aq. NaOH, (iii) Zn, aq. NaOH
3: H2SO4
4: LiAlH4
5: PBr3
6: PhLi
7: Rh-Al2O3 / 302 - 306 °C
View Scheme
参考文献
Karnes,H.A. et al.
Journal of the American Chemical Society, 1965 , vol. 87, # 24 p. 5554 - 5558
反应条件
1: PhLi
2: Rh-Al2O3 / 302 - 306 °C
View Scheme
参考文献
Karnes,H.A. et al.
Journal of the American Chemical Society, 1965 , vol. 87, # 24 p. 5554 - 5558
反应条件
1: LiAlH4
2: PBr3
3: PhLi
4: Rh-Al2O3 / 302 - 306 °C
View Scheme
参考文献
Karnes,H.A. et al.
Journal of the American Chemical Society, 1965 , vol. 87, # 24 p. 5554 - 5558
反应条件
sodium amide in ammonia
参考文献
Newman,M.S.; Lilje,K.C.
Journal of Organic Chemistry, 1979 , vol. 44, # 26 p. 4944 - 4946
