反应条件
1: 1.) AlCl3, 2.) K2CO3 / 1.) nitrobenzene a) 3 h, ice-bath temperature raising to 30 deg C, b) 3 h, 30 - 40 deg C, 2.) acetone, 12 h, reflux 2: 76 percent / anhydrous AlCl3 / benzene / 1.) 8 h, 65 deg C, 2.) overnight, room temperature 3: 79 percent / HCl, activated zinc dust / diethyl ether / 1.) during addition, 5 deg C, 2.) 3 h, 0 deg C 4: 1.) Mg / 1.) ether, 2.) a) room temperature, b) 1 h, reflux 5: 80 percent / toluene-p-sulphonic acid / benzene / 6 h / Heating View Scheme
参考文献
Murali, D.; Rao, G. S. Krishna
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 11 p. 1033 - 1034
