2-(4-(溴甲基)苯基)乙酸乙酯合成路线 (共 3 条)
反应条件
sulfuric acid
24 h; Inert atmosphere;
参考文献
Hammond, Nicholas L.; Choi, Seoung-Ryoung; Carvalho, Paulo; Liu, Hua; Khan, Shabana; Avery, Mitchell A.
Medicinal Chemistry Research, 2011 , vol. 20, # 4 p. 401 - 407
反应条件
1,3-dibromo-5,5-dimethyl-hydantoin; 2,2'-azo-bisisobutyronitrile in tetrachloromethane
T=60°C; 18 h; Yield given. Yields of byproduct given;
参考文献
Laurent, Eliane; Marquet, Bernard; Tardivel, Robert
Tetrahedron, 1991 , vol. 47, # 24 p. 3969 - 3980
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; sodium carbonate in acetic acid
参考文献
Merck Patent Gesellschaft Mit Beschrankter Haftung
Patent: US6028080 A1, 2000 ;