反应条件
1: 89.6 percent / HNO3, fuming sulfuric acid (30percent SO3) / 1.) 25-30 deg C, 2.) 85 deg C, 3.) 95 deg C, 4.5 h
2: 99.2 percent / conc. H2SO4 / 1.) 4 h, reflux, 2.) 25 deg C, 12-15 h
3: 84.6 percent / copper powder / xylene / Heating; 1.) 2 h, 2.) 1 h
4: 85 percent / 1.) 96percent H2SO4, 2.) H2O / 1.) 70 deg C, 2.) 95 deg C, 1h
5: 1.) oleum (20percent SO3), 2.) sodium azide
6: 23.4 percent / HNO3, H2SO4 / 1.) 30-35 deg C, 1.5 h, 2.) 65 deg C, 30 min, 3.) 70 deg C, 1.5 h
7: 38.6 percent / oleum (30percent SO3), H2O2 / 1.) 8-12 deg C, 1 h, 2.) 14 d, 25 deg C
View Scheme
参考文献
Nielsen, Arnold T.; Norris, William P.; Atkins, Ronald L.; Vuono, William R.
Journal of Organic Chemistry, 1983 , vol. 48, # 7 p. 1056 - 1059
