N,N'-二苯基-1,4-苯二胺合成路线 （共 58 条）
反应条件
1: With hydrogenchloride; anhydrous iron chloride in water 2 h; 2: With hydrazine
参考文献
Wang, Yue; Tran, Henry D.; Liao, Lei; Duan, Xiangfeng; Kaner, Richard B.
Journal of the American Chemical Society, 2010 , vol. 132, # 30 p. 10365 - 10373
反应条件
trichloromelamine; silica gel; sodium nitrite in dichloromethane; water T=20°C; 0.416667 h;
参考文献
Bamoniri; Zolfigol; Mirjalili; Fallah
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 9 p. 1393 - 1396
反应条件
trichloromelamine; silica gel; sodium nitrite in dichloromethane; water T=20°C; 0.5 h;
参考文献
Bamoniri; Zolfigol; Mirjalili; Fallah
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 9 p. 1393 - 1396
反应条件
in chlorobenzene T=298°C; Kinetics; Further Variations:Temperatures;
参考文献
Russian Chemical Bulletin, , vol. 55, # 10 p. 1723 - 1728
反应条件
in xylene at reflux 140-106°C for 165 h, then distilling butanol-borane azeotrop;
参考文献
Gmelin Handbook: B: B-Verb.1, 3.5.4.4, page 260 - 263
Full Text Show Details
U.S. Borax & Chemical Corp.
Patent: US3159590 , 1964 ;
C.A., 1965 , vol. 62, p. 11932
反应条件
acetic acid; platinum T=120°C; P=1471.02 Torr; Hydrogenation;
参考文献
U.S.Rubber Co.
Patent: US2276957 , 1941 ;
反应条件
1: N,N'-diphenyl-1,4-phenylenediamine With methyllithium T=-78°C; 2: methyl iodide T=-60°C;
参考文献
Flatt, Austen K.; Tour, James M.
Tetrahedron Letters, 2003 , vol. 44, # 35 p. 6699 - 6702
反应条件
NaBH4CN; acetic acid T=20°C; Methylation; reduction; 2.5 h;
参考文献
Chakrabarty; Batabyal; Khasnobis
Synthetic Communications, 2000 , vol. 30, # 20 p. 3651 - 3668
反应条件
100 deg C (30 min), ->180 deg C (1 h), 180 deg C, 30 min;
参考文献
Weller; Grellmann
Journal of the American Chemical Society, 1983 , vol. 105, # 20 p. 6268 - 6273
反应条件
MPPA in tetrahydrofuran
T=25°C;
参考文献
Zupancic, Joseph J.; Horn, Keith A.; Schuster, Gary B.
Journal of the American Chemical Society, 1980 , vol. 102, # 16 p. 5279 - 5285
