in deuterated toluene Kinetics; byproducts: Me2AsH, Me2AsAsMe2, (MeAs)5; -10°C, 40 h; not isolated, reaction followed by (11)B- and (13)C-NMR spectroscopy;
in neat (no solvent) prepared by condensing diborane in small portions to the amine until anexcess of diborane is present as indicated by the vapour pressure; detected by (13)C-NMR;
参考文献
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, , vol. 43, # 11 p. 1331 - 1336
