1: ethyl bromide With magnesium in diethyl ether
Grignard reaction;
2: 1-phenyl-propane-1,2-dione in diethyl ether
Grignard reaction; Title compound not separated from byproducts;
参考文献
Brunner, Henri; Stoehr, Frank
European Journal of Organic Chemistry, 2000 , # 15 p. 2777 - 2786
methanol
2 h; Heating; Yield given. Yields of byproduct given;
参考文献
Arbuzov, B. A.; Vizel', A. O.; Shchukina, L. I.; Giniyatullin, R. S.
Doklady Chemistry, 1980 , vol. 253, p. 371 - 374
Dokl. Akad. Nauk SSSR Ser. Khim., 1980 , vol. 253, # 4 p. 879 - 883
1: 2,4,6-trimethyl-1,3,5-triazine With potassium hydride in ethylene glycol dimethyl ether
T=20°C; 48 h;
2: ethyl bromide in ethylene glycol dimethyl ether
Further stages.;
参考文献
Nyquist, H. LeRoy; Beeloo, Edward A.; Hurlbut, Lydia S.; Watson-Clark, Rachel; Harwell, David E.
Journal of Organic Chemistry, 2002 , vol. 67, # 10 p. 3202 - 3212
