5-羟基-6,7-二甲氧基黄酮合成路线 （共 18 条）
反应条件
1: 0.15 g / selenium dioxide / pentan-1-ol / 24 h / Heating
2: 0.27 g / AlCl3 / acetonitrile / 24 h / Heating
View Scheme
参考文献
Parmar, Virinder S.; Gupta, Sandhya; Sinha, Rita; Sharma, Sunil K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 2 p. 244 - 256
反应条件
1: 0.35 g / aq. KOH / ethanol / 24 h / 30 °C
2: 0.15 g / selenium dioxide / pentan-1-ol / 24 h / Heating
3: 0.27 g / AlCl3 / acetonitrile / 24 h / Heating
View Scheme
参考文献
Parmar, Virinder S.; Gupta, Sandhya; Sinha, Rita; Sharma, Sunil K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 2 p. 244 - 256
反应条件
O-methyl transferase from cell-free extract of Citrus mitis; [methyl-14C]-S-adenosyl-L-methionine; 2-hydroxyethanethiol in water; dimethyl sulfoxide
T=35°C; 0.5 h; pH 7.5 buffer; Product distribution;
参考文献
Brunet, Gunter; Ibrahim, Ragai K.
Phytochemistry (Elsevier), 1980 , vol. 19, p. 741 - 746
参考文献
Bargellini
Gazzetta Chimica Italiana, 1919 , vol. 49 II, p. 57
反应条件
diethyl ether; acetone
参考文献
Shah et al.
Journal of the Chemical Society, 1936 , p. 591
反应条件
potassium carbonate; acetone
参考文献
Murti et al.
Proceedings - Indian Academy of Sciences, Section A, 1947 , # 26 p. 182,186
参考文献
Shah et al.
Journal of the Chemical Society, 1936 , p. 591
反应条件
sodium hydroxide; potassium peroxomonosulphate in water
T=15 - 20°C; Elbs persulfate oxidation;
参考文献
Gao, Hong; Nishioka, Tetsuo; Kawabata, Jun; Kasai, Takanori
Bioscience, Biotechnology and Biochemistry, 2004 , vol. 68, # 2 p. 369 - 375
