3-甲基-喹啉-2-甲酸合成路线 （共 10 条）
反应条件
1: With sodium hydroxide; water in methanol 0.5 h; 2: With hydrogenchloride in methanol; water
参考文献
Pfizer Inc
Patent: US2005/43292 A1, 2005 ;
Location in patent: Page/Page column 12 ;
反应条件
potassium permanganate; sulfuric acid in pyridine; water 24 h;
参考文献
Kepez, Mustafa
Monatshefte fuer Chemie, 1989 , vol. 120, p. 127 - 130
反应条件
1: 41 percent / SeO2 / ethyl acetate / 1 h / 60 °C 2: 66 percent / KMnO4, aq. H2SO4 / pyridine; H2O / 24 h View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 120, p. 127 - 130
反应条件
1: 24.2 g / triethylamine / ethanol / 2 h / 40 - 45 °C 2: Na2S2O4 / aq. ethanol / 3 h / Heating 3: aq. NaOH / 3 h / Heating View Scheme
参考文献
Heterocyclic Communications, , vol. 13, # 1 p. 49 - 56
反应条件
1: Na2S2O4 / aq. ethanol / 3 h / Heating 2: aq. NaOH / 3 h / Heating View Scheme
参考文献
Heterocyclic Communications, , vol. 13, # 1 p. 49 - 56
反应条件
1: 32 g / sodium hypochlorite; potassium hydroxide / aq. ethanol / 0 °C 2: 24.2 g / triethylamine / ethanol / 2 h / 40 - 45 °C 3: Na2S2O4 / aq. ethanol / 3 h / Heating 4: aq. NaOH / 3 h / Heating View Scheme
参考文献
Heterocyclic Communications, , vol. 13, # 1 p. 49 - 56
反应条件
sodium hydroxide 3 h; Heating;
参考文献
Heterocyclic Communications, , vol. 13, # 1 p. 49 - 56
反应条件
selenium(IV) oxide; m-xylene
参考文献
Chemische Berichte, , vol. 84, p. 477
反应条件
anhydrous calcium nitrate in methanol T=30°C; 8 h; without Ca(NO3)2, other acetoacetamides; Product distribution;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 331, # 5 p. 736 - 744
参考文献
Chemische Berichte, , vol. 84, p. 477
