4-甲基-4-苯基-2-戊酮合成路线 (共 43 条)
反应条件
sodium acetate; antimony trichloride; palladium diacetate in acetic acid
T=25°C; 24 h;
参考文献
Cho, Chan Sik; Motofusa, Shin-ichi; Ohe, Kouichi; Uemura, Sakae; Shim, Sang Chul
Journal of Organic Chemistry, 1995 , vol. 60, # 4 p. 883 - 888
反应条件
tetrabutyl ammonium fluoride; antimony trichloride; acetic acid; palladium diacetate in acetonitrile
T=60°C; 30 h;
参考文献
Denmark, Scott E.; Amishiro, Nobuyoshi
Journal of Organic Chemistry, 2003 , vol. 68, # 18 p. 6997 - 7003
反应条件
(lithium)2(CN)(phenyl)2cuprate in diethyl ether
T=-78°C; 1 h; other solvents; Product distribution;
参考文献
Lipshutz, Bruce H.; Wilhelm, Robert S.; Kozlowski, Joseph A.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 3938 - 3942
反应条件
[2,2']bipyridinyl; palladium diacetate in methanol
T=80°C; in a sealed tube;
参考文献
Lin, Shaohui; Lu, Xiyan
Organic Letters, 2010 , vol. 12, # 11 p. 2536 - 2539
反应条件
(i) CuBr*Me2S, Me2S, Et2O, (ii) /BRN= 1361550/; Multistep reaction;
参考文献
House,H.O.; Wilkins,J.M.
Journal of Organic Chemistry, 1978 , vol. 43, p. 2443 - 2454
反应条件
silver(I) acetate; palladium diacetate in acetic acid
T=25°C; 24 h;
参考文献
Cho, Chan Sik; Tanabe, Koichiro; Uemura, Sakae
Tetrahedron Letters, 1994 , vol. 35, # 8 p. 1275 - 1278
反应条件
in tetrahydrofuran; diethyl ether
T=-78°C; 2 h;
参考文献
Lipshutz, Bruce H.; Ellsworth, Edmund L.; Siahaan, Teruna J.
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1351 - 1358
反应条件
palladium diacetate; silver(I) acetate; antimony trichloride; acetic acid
T=25°C; 24 h;
参考文献
Cho, Chan Sik; Motofusa, Shin-Ichi; Ohe, Kouichi; Uemura, Sakae
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 8 p. 2341 - 2348
反应条件
1: diethyl ether / Ambient temperature
2: aq. HCl
View Scheme
参考文献
Keuk,B.P. et al.
Synthesis, 1977 , p. 638 - 640
反应条件
1: diethyl ether / Ambient temperature
2: aq. HCl
View Scheme
参考文献
Keuk,B.P. et al.
Synthesis, 1977 , p. 638 - 640