二(丙-2-烯氧基)磷酰基甲基苯合成路线 （共 6 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); dimedone in tetrahydrofuran T=20°C; 1.5 h;
参考文献
Bhattacharya, Asish K; Stolz, Florian; Kurzeck, Juergen; Rueger, Wolfgang; Schmidt, Richard R
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 4 p. 1129 - 1136
反应条件
in toluene
T=95°C; 4 h;
参考文献
Bhattacharya, Asish K; Stolz, Florian; Kurzeck, Juergen; Rueger, Wolfgang; Schmidt, Richard R
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 4 p. 1129 - 1136
参考文献
Toy; Cooper
Journal of the American Chemical Society, 1954 , vol. 76, p. 2191,2194
反应条件
1: 3 h / 0 °C
2: (COCl)2; DMF / CH2Cl2 / 1 h / 20 °C
3: 1.37 g / pyridine; DMAP / CH2Cl2 / -20 - 20 °C
View Scheme
参考文献
Skropeta, Danielle; Schmidt, Richard R.
Tetrahedron Asymmetry, 2003 , vol. 14, # 2 p. 265 - 273
反应条件
1: (COCl)2; DMF / CH2Cl2 / 1 h / 20 °C
2: 1.37 g / pyridine; DMAP / CH2Cl2 / -20 - 20 °C
View Scheme
参考文献
Skropeta, Danielle; Schmidt, Richard R.
Tetrahedron Asymmetry, 2003 , vol. 14, # 2 p. 265 - 273
参考文献
Shell Devel. Co.
Patent: US2601520 , 1949 ;
