2-羟基-6-巯基-5-甲基-4-嘧啶羧酸合成路线 (共 3 条)
反应条件
potassium hydroxide in methanol
1 h; Ambient temperature;
参考文献
Batty, Craig A.; Manthey, Michael K.; Kirk, Julie; Manthey, Monika; Christopherson, Richard I.; Hambley, Trevor
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 4 p. 1355 - 1367
反应条件
1: 66 percent / Cs2CO3 / dimethylformamide
2: 69 percent / P2S5 / dioxane / 24 h / Heating
3: 65 percent / aq. KOH / methanol / 1 h / Ambient temperature
View Scheme
参考文献
Batty, Craig A.; Manthey, Michael K.; Kirk, Julie; Manthey, Monika; Christopherson, Richard I.; Hambley, Trevor
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 4 p. 1355 - 1367
反应条件
1: 69 percent / P2S5 / dioxane / 24 h / Heating
2: 65 percent / aq. KOH / methanol / 1 h / Ambient temperature
View Scheme
参考文献
Batty, Craig A.; Manthey, Michael K.; Kirk, Julie; Manthey, Monika; Christopherson, Richard I.; Hambley, Trevor
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 4 p. 1355 - 1367