N,N'-二琥珀酰亚胺基碳酸酯合成路线 (共 77 条)
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane; acetonitrile 6 h; Ambient temperature;
参考文献
Sawayama; Tsukamoto; Sasagawa; Nishimura; Deguchi; Takeyama; Hosoki
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 1 p. 110 - 115
反应条件
in toluene 18 h; Ambient temperature;
参考文献
Harada; Morie; Hirokawa; Terauchi; Fujiwara; Yoshida; Kato
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 11 p. 1912 - 1930
反应条件
4-(N,N-dimethlyamino)pyridine in ethyl acetate; N,N-dimethyl-formamide; toluene
参考文献
Sas, Benedikt; Eycken, Johan Van der; Van hemel, Johan; Blom, Petra; Vandenkerckhove, Jan; Ruttens, Bart
Patent: US2003/158243 A1, 2003 ;
反应条件
triethylamine in dichloromethane; acetonitrile
参考文献
Laboratoires Hoechst; Behringwerke A.G.
Patent: US5561119 A1, 1996 ;
反应条件
in chloroform 12 h; Heating / reflux;
参考文献
AMGEN INC.
Patent: WO2004/35549 A1, 2004 ;
Location in patent: Page 200 ;
WO 2004/035549 A1
参考文献
Ogura, Haruo; Takeda, Kazuyoshi
Heterocycles, 1981 , vol. 15, # 1 p. 467 - 468
反应条件
triethylamine in acetonitrile Ambient temperature;
参考文献
Takeda, Kazuyoshi; Akagi, Yoshie; Saiki, Atsuko; Tsukahara, Toshiko; Ogura, Haruo
Tetrahedron Letters, 1983 , vol. 24, # 42 p. 4569 - 4572
反应条件
triethylamine in acetonitrile T=23°C; 7 h;
参考文献
Ghosh, Arun K.; Leshchenko, Sofiya; Noetzel, Marcus
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 7822 - 7829
反应条件
1: vinyl acetate; (3aS,6aR)-hexahydrofuro[2,3-b]furan-3-ol in dichloromethane; tert-butyl methyl ether T=20°C; 5 h; Resolution of racemateLarge scale reactionEnzymatic reaction; 2: N,N'-disuccinimidyl-carbonate With triethylamine in acetonitrile T=20°C; 24 h; enantioselective reaction;
参考文献
Khmelnitsky, Yuri L.; Michels, Peter C.; Cotterill, Ian C.; Eissenstat, Michael; Sunku, Venkataiah; Veeramaneni, Venugopal R.; Cittineni, Hariprasad; Kotha, Gopal R.; Talasani, Shyamsunder R.; Ramanathan, Krishna K.; Chitineni, Vakula K.; Venepalli, Bhaskar R.
Organic Process Research and Development, 2011 , vol. 15, # 1 p. 279 - 283
反应条件
in acetonitrile Ambient temperature;
参考文献
Takeda, Kazuyoshi; Akagi, Yoshie; Saiki, Atsuko; Tsukahara, Toshiko; Ogura, Haruo
Tetrahedron Letters, 1983 , vol. 24, # 42 p. 4569 - 4572