您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
74133-16-7
合成路线
（共 8 条）
166373-40-6
→
反应条件
74133-16-7
反应条件
(+/-)-trans-2-(butylsulfonyl)-3-phenyloxaziridine in dichloromethane 0.666667 h;
参考文献
Kuehne, Paul; Linden, Anthony; Hesse, Manfred
Helvetica Chimica Acta, 1996 , vol. 79, # 4 p. 1085 - 1094
3646-50-2
DL-3-氨基-3-苯基丙酸
→
反应条件
74133-16-7
反应条件
1: HCl gas / 1 h / Heating 2: 93 percent / 3 h / 125 - 135 °C 3: 31 percent / NaBH3CN / acetic acid / 1 h / 50 °C / before heating 2 h, after heating 23 h room temperature 4: 83 percent / NaOEt / toluene / 5 h 5: 87 percent / hydrogen / Raney Ni / aq. NH3; aq. ethanol / 14 h / 2585.7 Torr 6: 88 percent / NaOH / aq. ethanol / 264 h / 55 °C 7: 68 percent / (+/-)-trans-2-(butylsulfonyl)-3-phenyloxaziridine / CH2Cl2 / 0.67 h View Scheme
参考文献
Kuehne, Paul; Linden, Anthony; Hesse, Manfred
Helvetica Chimica Acta, 1996 , vol. 79, # 4 p. 1085 - 1094
37088-66-7
(S)-3-氨基-3-苯基丙酸甲酯
→
反应条件
74133-16-7
反应条件
1: 93 percent / 3 h / 125 - 135 °C 2: 31 percent / NaBH3CN / acetic acid / 1 h / 50 °C / before heating 2 h, after heating 23 h room temperature 3: 83 percent / NaOEt / toluene / 5 h 4: 87 percent / hydrogen / Raney Ni / aq. NH3; aq. ethanol / 14 h / 2585.7 Torr 5: 88 percent / NaOH / aq. ethanol / 264 h / 55 °C 6: 68 percent / (+/-)-trans-2-(butylsulfonyl)-3-phenyloxaziridine / CH2Cl2 / 0.67 h View Scheme
参考文献
Kuehne, Paul; Linden, Anthony; Hesse, Manfred
Helvetica Chimica Acta, 1996 , vol. 79, # 4 p. 1085 - 1094
112020-25-4
→
反应条件
74133-16-7
反应条件
1: 83 percent / NaOEt / toluene / 5 h 2: 87 percent / hydrogen / Raney Ni / aq. NH3; aq. ethanol / 14 h / 2585.7 Torr 3: 88 percent / NaOH / aq. ethanol / 264 h / 55 °C 4: 68 percent / (+/-)-trans-2-(butylsulfonyl)-3-phenyloxaziridine / CH2Cl2 / 0.67 h View Scheme
参考文献
Kuehne, Paul; Linden, Anthony; Hesse, Manfred
Helvetica Chimica Acta, 1996 , vol. 79, # 4 p. 1085 - 1094
100-52-7
苯甲醛
→
反应条件
74133-16-7
反应条件
1: 56 percent / ammonium acetate / ethanol / 6.5 h / Heating 2: HCl gas / 1 h / Heating 3: 93 percent / 3 h / 125 - 135 °C 4: 31 percent / NaBH3CN / acetic acid / 1 h / 50 °C / before heating 2 h, after heating 23 h room temperature 5: 83 percent / NaOEt / toluene / 5 h 6: 87 percent / hydrogen / Raney Ni / aq. NH3; aq. ethanol / 14 h / 2585.7 Torr 7: 88 percent / NaOH / aq. ethanol / 264 h / 55 °C 8: 68 percent / (+/-)-trans-2-(butylsulfonyl)-3-phenyloxaziridine / CH2Cl2 / 0.67 h View Scheme
参考文献
Kuehne, Paul; Linden, Anthony; Hesse, Manfred
Helvetica Chimica Acta, 1996 , vol. 79, # 4 p. 1085 - 1094
112020-24-3
→
反应条件
74133-16-7
反应条件
1: 31 percent / NaBH3CN / acetic acid / 1 h / 50 °C / before heating 2 h, after heating 23 h room temperature 2: 83 percent / NaOEt / toluene / 5 h 3: 87 percent / hydrogen / Raney Ni / aq. NH3; aq. ethanol / 14 h / 2585.7 Torr 4: 88 percent / NaOH / aq. ethanol / 264 h / 55 °C 5: 68 percent / (+/-)-trans-2-(butylsulfonyl)-3-phenyloxaziridine / CH2Cl2 / 0.67 h View Scheme
参考文献
Kuehne, Paul; Linden, Anthony; Hesse, Manfred
Helvetica Chimica Acta, 1996 , vol. 79, # 4 p. 1085 - 1094
180324-14-5
→
反应条件
74133-16-7
反应条件
1: 87 percent / hydrogen / Raney Ni / aq. NH3; aq. ethanol / 14 h / 2585.7 Torr 2: 88 percent / NaOH / aq. ethanol / 264 h / 55 °C 3: 68 percent / (+/-)-trans-2-(butylsulfonyl)-3-phenyloxaziridine / CH2Cl2 / 0.67 h View Scheme
参考文献
Kuehne, Paul; Linden, Anthony; Hesse, Manfred
Helvetica Chimica Acta, 1996 , vol. 79, # 4 p. 1085 - 1094
180324-13-4
→
反应条件
74133-16-7
反应条件
1: 88 percent / NaOH / aq. ethanol / 264 h / 55 °C 2: 68 percent / (+/-)-trans-2-(butylsulfonyl)-3-phenyloxaziridine / CH2Cl2 / 0.67 h View Scheme
参考文献
Kuehne, Paul; Linden, Anthony; Hesse, Manfred
Helvetica Chimica Acta, 1996 , vol. 79, # 4 p. 1085 - 1094
