1-(2-甲氧基苯基)乙醇合成路线 （共 37 条）
反应条件
1: PBr3 3: ethanolic KOH-solution 4: hydrobromic acid View Scheme
参考文献
Ramart-Lucas; Hoch
Bulletin de la Societe Chimique de France, 1935 , vol. <5> 2, p. 327,333
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1935 , vol. 201, p. 1387
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite in acetonitrile T=35°C; pH 6.7;
参考文献
Zhao; Li; Mano; Song; Tschaen; Grabowski; Reider
Journal of Organic Chemistry, 1999 , vol. 64, # 7 p. 2564 - 2566
反应条件
molecular sieve; pyridinium chlorochromate in dichloromethane T=20°C; 8 h;
参考文献
Fernandes, Rodney A.; Kumar, Pradeep
Tetrahedron Letters, 2003 , vol. 44, # 6 p. 1275 - 1278
反应条件
1: PBr3 3: ethanolic KOH-solution View Scheme
参考文献
Ramart-Lucas; Hoch
Bulletin de la Societe Chimique de France, 1935 , vol. <5> 2, p. 327,333
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1935 , vol. 201, p. 1387
反应条件
potassium hydroxide T=225°C; P=12 Torr;
参考文献
Marvel; Hein
Journal of the American Chemical Society, 1948 , vol. 70, p. 1895,1897
反应条件
thionyl chloride in benzene T=50°C; 2 h;
参考文献
Kato; Takemoto; Achiwa
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 11 p. 2003 - 2006
反应条件
1: pyridinium chlorochromate / dichloromethane 2: sodium hydride / tetrahydrofuran 3: hydrogen; palladium on activated charcoal / ethyl acetate View Scheme
参考文献
Mimori, Seisuke; Okuma, Yasunobu; Kaneko, Masayuki; Kawada, Koichi; Nomura, Yasuyuki; Murakami, Yasuoki; Hamana, Hiroshi
Chemistry Letters, 2013 , vol. 42, # 9 p. 1051 - 1052
反应条件
phosphorus tribromide 1 h; Heating;
参考文献
Anderson; Bussolotti; Coward
Journal of Medicinal Chemistry, 1981 , vol. 24, # 11 p. 1271 - 1277
反应条件
triphenylphosphine in hexane; dichloromethane; ethyl acetate
参考文献
Fujisawa Pharmaceutical Co., Ltd.
Patent: US6582351 B1, 2003 ;
反应条件
lithium bromide in dichloromethane; acetone
参考文献
Merck and Co., Inc.
Patent: US6100293 A1, 2000 ;
