2-(叔丁基二甲基硅杂氧基)环己酮合成路线 (共 13 条)
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemische Berichte, , vol. 113, # 4 p. 1245 - 1263
反应条件
triphenylphosphine; isopropyl alcohol; Wilkinson's catalyst in 1,4-dioxane
T=60°C; 4 h;
参考文献
Lebel, Helene; Guay, Danielle; Paquet, Valerie; Huard, Kim
Organic Letters, 2004 , vol. 6, # 18 p. 3047 - 3050
反应条件
1: Methyltriphenylphosphonium bromide With sodium hexamethyldisilazane in 1,4-dioxane
T=60°C; Wittig reaction; 1 h;
2: 2-(tert-Butyldimethylsilyloxy)-1-cyclohexanon in 1,4-dioxane
T=60°C; Wittig reaction; 4 h;
参考文献
Lebel, Helene; Guay, Danielle; Paquet, Valerie; Huard, Kim
Organic Letters, 2004 , vol. 6, # 18 p. 3047 - 3050