4-(四氢-吡喃-2-基氧基)-苯甲醛合成路线 (共 29 条)
反应条件
pyridinium p-toluenesulfonate in dichloromethane 1.5 h; Ambient temperature;
参考文献
Pez, Didier; Leal, Isabel; Zuccotto, Fabio; Boussard, Cyrille; Brun, Reto; Croft, Simon L.; Yardley, Vanessa; Ruiz Perez, Luis M.; Gonzalez Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4693 - 4711
反应条件
3,5-dimethylpyrazolium fluorochromate(VI) T=20°C; 0.0666667 h;
参考文献
Chaudhuri; Dehury; Hussain; Duarah; Gogoi
Organic Preparations and Procedures International, 2006 , vol. 38, # 3 p. 331 - 336
反应条件
pyridinium p-toluenesulfonate; sodium hydrogencarbonate in dichloromethane
反应条件
pyridinium p-toluenesulfonate in dichloromethane T=20°C; 4 h;
参考文献
European Journal of Pharmaceutical Sciences, , vol. 35, # 4 p. 293 - 306
反应条件
pyridinium p-toluenesulfonate in dichloromethane T=20°C;
参考文献
European Journal of Medicinal Chemistry, , vol. 44, # 2 p. 915 - 919
反应条件
1: With potassium hydroxide in ethanol T=20°C; 12 h; 2: With hydrogenchloride; water in ethanol T=20°C; 4 h;
参考文献
Lee, Chong-Yew; Chew, Eng-Hui; Go, Mei-Lin
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 7 p. 2957 - 2971
反应条件
boron trifluoride diethyl etherate; sodium cyanoborohydride in tetrahydrofuran 8 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Srikrishna, A.; Sattigeri, J. A.; Viswajanani, R.; Yelamaggad, C. V.
Journal of Organic Chemistry, 1995 , vol. 60, # 7 p. 2260
反应条件
1: barium hydroxide octahydrate / methanol / 2 h / 50 °C 2: p-toluenesulfonic acid / methanol / 15 h / Ambient temperature View Scheme
参考文献
Artico, Marino; Santo, Roberte Di; Costi, Roberta; Novellino, Ettore; Greco, Giovanni; Massa, Silvio; Tramontane, Enzo; Marongiu, Maria E.; De Montis, Antonella; Colla, Paolo La
Journal of Medicinal Chemistry, 1998 , vol. 41, # 21 p. 3948 - 3960
反应条件
1.1: 71 percent / NaOEt / ethanol / 24 h / Heating 2.1: NaOEt / ethanol / 0.08 h 2.2: 32 percent / ethanol / 24 h / Heating 3.1: 100 percent / hydrochloric acid / methanol / 2 h / 20 °C View Scheme
参考文献
Pez, Didier; Leal, Isabel; Zuccotto, Fabio; Boussard, Cyrille; Brun, Reto; Croft, Simon L.; Yardley, Vanessa; Ruiz Perez, Luis M.; Gonzalez Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4693 - 4711
反应条件
1: Ba(OH)2*8H2O / methanol / 12 h / 40 °C 2: p-TsOH / methanol / 3 h / Ambient temperature View Scheme
参考文献
Sogawa; Nihro; Ueda; Izumi; Miki; Matsumoto; Satoh
Journal of Medicinal Chemistry, 1993 , vol. 36, # 24 p. 3904 - 3909