顺式-十氢-1H,6H-3α,5α,8α,10α-四氮杂芘合成路线 (共 5 条)
反应条件
in methanol; water T=20°C; 3 h;
参考文献
Le Baccon; Chuburu; Toupet; Handel; Soibinet; Dechamps-Olivier; Barbier; Aplincourt
New Journal of Chemistry, 2001 , vol. 25, # 9 p. 1168 - 1174
反应条件
1: 100 percent / acetonitrile / 168 h / 20 °C 2: 93 percent / hydroxylamine hydrochloride; sodium ethoxide / ethanol / 4 h / Heating View Scheme
参考文献
Le Baccon; Chuburu; Toupet; Handel; Soibinet; Dechamps-Olivier; Barbier; Aplincourt
New Journal of Chemistry, 2001 , vol. 25, # 9 p. 1168 - 1174
反应条件
1: 90 percent / acetonitrile / 0.25 h / 20 °C 2: NH2OH / ethanol / 3 h / Heating View Scheme
参考文献
Kotek, Jan; Hermann, Petr; Vojtisek, Pavel; Rohovec, Jan; Lukes, Ivan
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 2 p. 243 - 266
反应条件
1: acetonitrile / Ambient temperature View Scheme
参考文献
Weisman, Gary R.; Wong, Edward H.; Hill, Daniel C.; Rogers, Mark E.; Reed, David P.; Calabrese, Joseph C.
Chemical Communications, 1996 , # 8 p. 947 - 948
反应条件
1: 65 percent / acetonitrile / 72 h 2: H2O; NaOH / 2 h View Scheme
参考文献
Kotek, Jan; Hermann, Petr; Vojtisek, Pavel; Rohovec, Jan; Lukes, Ivan
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 2 p. 243 - 266