5-甲基-2-苯基苯并恶唑合成路线 （共 48 条）
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
P=4912.9 Torr; a.) 155-160 deg C, 16 h, b.) 210 deg C, 3 d;
参考文献
Perry, Robert J.; Wilson, B. David
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6351 - 6354
反应条件
tin(ll) chloride in 1,4-dioxane
T=180°C; 30 h;
参考文献
Cho, Chan Sik; Kim, Dong Tak; Zhang, Jiao Qiang; Ho, Son-Lam; Kim, Tae-Jeong; Shim, Sang Chul
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 2 p. 421 - 423
反应条件
copper(l) iodide; oxygen; palladium diacetate; potassium carbonate in 1,4-dioxane
T=120°C; 48 h; Sealed tube;
参考文献
Zhang, Manli; Zhang, Shouhui; Liu, Miaochang; Cheng, Jiang
Chemical Communications, 2011 , vol. 47, # 41 p. 11522 - 11524
反应条件
Ru(phen)3(Cl)2; oxygen in dimethyl sulfoxide
T=32°C; 36 h; IrradiationSchlenk technique;
参考文献
Liu, Jie; Liu, Qiang; Yi, Hong; Qin, Chu; Bai, Ruopeng; Qi, Xiaotian; Lan, Yu; Lei, Aiwen
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 502 - 506
Angew. Chem., 2014 , vol. 126, # 2 p. 512 - 516,5
反应条件
caesium carbonate; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide
T=100°C; Kinetics;
参考文献
Sanchez, Rafael S.; Zhuravlev, Fedor A.
Journal of the American Chemical Society, 2007 , vol. 129, # 18 p. 5824 - 5825
反应条件
1: DBU / PdCl2(PPh3)2, PPh3 / toluene / 1.25 h / 120 °C / 4654.3 Torr
2: methanesulfonic acid / toluene / 2 h / Heating
View Scheme
参考文献
Perry, Robert J.; Wilson, B. David; Miller, Richard J.
Journal of Organic Chemistry, 1992 , vol. 57, # 10 p. 2883 - 2887
反应条件
potassium phosphate; oxygen; palladium diacetate; copper(ll) bromide; 2,2,2-trimethylacetic acid in N,N-dimethyl acetamide
T=120°C; P=760.051 Torr; 6 h;
参考文献
Wu, Ge; Zhou, Jun; Zhang, Min; Hu, Peng; Su, Weiping
Chemical Communications, 2012 , vol. 48, # 71 p. 8964 - 8966
反应条件
triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene
17 h; Reflux;
参考文献
Xu, Quancai; Li, Zhengning; Chen, Huiying
Chinese Journal of Chemistry, 2011 , vol. 29, # 5 p. 925 - 932
反应条件
1: methanol / 3 h / Heating
2: 96 percent / O2; 4 Angstroem molecular sieves / [Co2L(μ-OH)] {H3L=2,6-bis[(2-OH-Ph)iminoMe]-4-Me-phenol} / dimethylformamide / 24 h / 90 °C / 680.3 Torr
View Scheme
参考文献
Chang, Shian Yuh; Cheng, Yee Hsing; Uang, Bing-Jium; Cheng, Cheu Pyeng
Journal of the Chemical Society - Dalton Transactions, 1999 , # 16 p. 2769 - 2776
反应条件
silica gel
0.0333333 h; microwave irradiation;
参考文献
Rostamizadeh; Derafshian
Journal of Chemical Research - Part S, 2001 , # 6 p. 227 - 228
