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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
74213-48-2
合成路线
（共 8 条）
74213-48-2
→
反应条件
14637-69-5
反应条件
1.1: palladium(II) acetate / diethyl ether / 1 h / 0 - 20 °C 1.2: KHF2 / methanol; H2O / 4 h / 20 °C 2.1: 88 percent / K3PO4*3H2O / tetrakis(triphenylphosphine)palladium(0) / toluene; H2O / 20 h / 100 °C View Scheme
参考文献
Fang, Guo-Hua; Yan, Zheng-Jun; Deng, Min-Zhi
Organic Letters, 2004 , vol. 6, # 3 p. 357 - 360
74213-48-2
→
反应条件
104-57-4
甲酸苄酯
+
122-78-1
苯乙醛
+
100-51-6
苯甲醇
反应条件
phosphite dehydrogenase; recombinant phenylacetone monooxygenase from Thermobifida fusca; NADPH in dimethyl sulfoxide T=30°C; 4 h; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
74213-48-2
→
反应条件
60-12-8
苯乙醇
+
122-78-1
苯乙醛
反应条件
4-hydroxyacetophenone monooxygenase from Pseudomonas fluorescens; phosphite dehydrogenase; NADPH in dimethyl sulfoxide T=24°C; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
74213-48-2
→
反应条件
100-51-6
苯甲醇
反应条件
phosphite dehydrogenase; recombinant phenylacetone monooxygenase from Thermobifida fusca; NADPH in dimethyl sulfoxide T=30°C; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
74213-48-2
→
反应条件
104-57-4
甲酸苄酯
+
122-78-1
苯乙醛
+
100-51-6
苯甲醇
反应条件
phosphite dehydrogenase; recombinant phenylacetone monooxygenase from Thermobifida fusca; NADPH in dimethyl sulfoxide T=30°C; 4 h; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
74213-48-2
→
反应条件
60-12-8
苯乙醇
+
122-78-1
苯乙醛
反应条件
4-hydroxyacetophenone monooxygenase from Pseudomonas fluorescens; phosphite dehydrogenase; NADPH in dimethyl sulfoxide T=24°C; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
74213-48-2
→
反应条件
122-78-1
苯乙醛
反应条件
4-hydroxyacetophenone monooxygenase from Pseudomonas fluorescens; phosphite dehydrogenase; NADPH in dimethyl sulfoxide T=24°C; 4 h; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
74213-48-2
→
反应条件
104-57-4
甲酸苄酯
+
122-78-1
苯乙醛
+
100-51-6
苯甲醇
反应条件
phosphite dehydrogenase; recombinant phenylacetone monooxygenase from Thermobifida fusca; NADPH in dimethyl sulfoxide T=30°C; 4 h; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
