1,1,1,3,5,5,5-七甲基-3-(3-缩水甘油醚氧基丙基)三硅氧烷合成路线 (共 8 条)
反应条件
1,2,3-trimethylimidazolium methylsulphate; [{Rh(μ-OSiMe3)(cod)}2] T=90°C; 2 h; Product distribution; Further Variations:CatalystsReagents;
参考文献
Marciniec, Bogdan; Maciejewski, Hieronim; Szubert, Karol; Kurdykowska, Magdalena
Monatshefte fur Chemie, 2006 , vol. 137, # 5 p. 605 - 611
反应条件
1: 2-methyl-2-propenoic acid With lithium hydroxide; 4-methoxy-phenol
T=80°C;
2: (3-glycidoxypropyl)bis(trimethylsiloxy)methylsilane T=20 - 90°C; 20 h; Product distribution / selectivity;
参考文献
Molock, Frank; Mahadevan, Shivkumar; Ward, Robert S.; Wang, Shanger; Parakka, James Paul; Tian, Yuan
Patent: US2006/47134 A1, 2006 ;
Location in patent: Page/Page column 6 ;
反应条件
water; 4-methoxy-phenol; methacrylic acid sodium salt
T=100°C; Product distribution / selectivity;
参考文献
TORAY INDUSTRIES, INC.
Patent: EP1719776 A1, 2006 ;
Location in patent: Page/Page column 10-11 ;
反应条件
4-methoxy-phenol
T=100°C;
参考文献
JOHNSON and JOHNSON VISION CARE, INC.; TORAY INDUSTRIES, INC.
Patent: WO2008/66758 A1, 2008 ;
Location in patent: Page/Page column 26-27 ;
反应条件
4-methoxy-phenol
T=90°C; 15 h; Conversion of starting material;
参考文献
JOHNSON and JOHNSON VISION CARE, INC.
Patent: WO2005/5445 A1, 2005 ;
Location in patent: Page/Page column 9 ;
反应条件
4-methoxy-phenol
T=90 - 100°C; 15 h; Conversion of starting material;
参考文献
JOHNSON and JOHNSON VISION CARE, INC.
Patent: WO2005/5445 A1, 2005 ;
Location in patent: Page/Page column 9 ;
反应条件
4-methoxy-phenol
T=90°C; 15 h; Conversion of starting material;
参考文献
JOHNSON and JOHNSON VISION CARE, INC.
Patent: WO2005/5445 A1, 2005 ;
Location in patent: Page/Page column 9 ;
反应条件
4-methoxy-phenol
T=90°C; 15 h; Product distribution / selectivity;
参考文献
Molock, Frank; Mahadevan, Shivkumar; Ward, Robert S.; Wang, Shanger; Parakka, James Paul; Tian, Yuan
Patent: US2006/47134 A1, 2006 ;
Location in patent: Page/Page column 4-5 ;